A kind of organic carboxylate nucleating agent and its preparation process
A technology of organic carboxylic acid and nucleating agent, applied in the field of organic carboxylate nucleating agent and its preparation technology, can solve the problems of poor dispersibility, poor application effect and the like, and achieve good dispersibility, good application effect and good stability effect of nucleation
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Embodiment 1
[0039] Embodiment 1: A kind of organic carboxylate nucleating agent, each component and its corresponding parts by weight are as shown in Table 1, and are prepared through the following steps:
[0040] Step 1, dissolve and mix the corresponding parts by weight of p-tert-butylbenzoic acid, water and n-butanol evenly for 0.5h, then add NaAlO 2 With the sodium hydroxide of 1 / 2 corresponding parts by weight, carry out neutralization reaction 0.6h;
[0041]Step 2, followed by adding the corresponding parts by weight of aluminum chloride hexahydrate, after reacting for 2 hours, press filtration to remove the hazardous waste liquid, and after circulating water washing for 3 times, then add the remaining parts by weight of sodium hydroxide, press filter Remove chloride ions to obtain a mixture;
[0042] Step 3: Add corresponding parts by weight of citric acid into the mixture, stir for 1.5 hours, distill under reduced pressure, and perform vacuum drying to obtain an organic carboxyla...
Embodiment 2-8
[0044] Example 2-8: An organic carboxylate nucleating agent, the difference from Example 1 is that each component and its corresponding parts by weight are shown in Table 1.
[0045] Each component and parts by weight thereof in table 1 embodiment 1-8
[0046]
Embodiment 9
[0047] Embodiment 9: a kind of organic carboxylate nucleating agent, the difference from embodiment 1 is that step one is specifically set as, the corresponding parts by weight are 130 parts of p-tert-butylbenzoic acid, 350 parts of Water and 90 parts of n-butanol are dissolved and mixed evenly, and the time is 0.5h, and then 20 parts of KAlO are added 2 And 9 parts of sodium hydroxide, carry out neutralization reaction 0.6h.
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Abstract
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