Shellac viscose, preparation method of shellac viscose and preparation method of bismuth telluride crystal grains
A technology of bismuth telluride and shellac, applied in the field of materials, can solve the problems of low preparation efficiency of semiconductor bismuth telluride crystal grains, easy generation of burrs, low cutting speed, etc., to achieve low cost, reduce burr generation, and improve quality and precision. Effect
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preparation example Construction
[0025] The preparation method of above-mentioned shellac viscose comprises the steps:
[0026] a, prepare the raw materials, according to the mass percentage, the shellac content is 40-44%, the dibutyl phthalate content is 7-9%, the diisooctyl phthalate content is 11-13%, and the talcum powder content is 35- 38% prepare raw materials;
[0027] b. Place the raw materials prepared in step a in a heating container for heating and melting, and stir with a smooth stir bar after melting;
[0028] c. Pour the mixed material evenly stirred in step b into a cooling container and cool to room temperature.
[0029] In step a, the shellac is preferably natural grade A shellac. In step b, the heating container is preferably a crucible, the heating and melting temperature of the raw material is 270-280° C., and the stirring is preferably a smooth glass rod. The cooling container is preferably a glass dish. The preparation method of the shellac viscose is simple in operation, the require...
Embodiment 1
[0041] A method for preparing bismuth telluride grains with a size of 2.1mm×1mm×1mm in the shape of a cuboid, wherein 2.1mm is the thickness, and 1mm is the length and width, comprising the following steps:
[0042]A. Prepare the base, 10 bismuth telluride wafers, and 8mm thick graphite pads. The shape of the bismuth telluride wafer is a cuboid, with a thickness of 2.1mm, a length of 10mm, and a width of 10mm;
[0043] B. The base, the bismuth telluride wafer, and the graphite pad are placed on a heating platform with a temperature of 235°C for heating, and the base and all the bismuth telluride wafers are stacked together from bottom to top through shellac adhesive bonding. After connecting, cool to room temperature for later use.
[0044] C, carry out cutting, at first base is stacked together, and all bismuth telluride wafers are fixed on the inner circle cutting machine and carry out the first side cutting, obtain semi-bismuth telluride grain, the length of semi-bismuth te...
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