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Preparation method and application of material for adsorption removal of organic matter and ammonia nitrogen

An organic matter, ammonia nitrogen technology, applied in chemical instruments and methods, adsorbed water/sewage treatment, water pollutants, etc., can solve the problems of lack of nitrogen removal adsorbents and high operating costs, and achieve the effect of alleviating water shortages

Inactive Publication Date: 2019-11-12
ANHUI MEIZIRAN ENVIRONMENTAL TECH
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Problems solved by technology

Therefore, how to reduce the concentration of ammonia nitrogen in non-drinking water sources in nature to the third type of surface water environmental standard, which is less than 1mg / l, is a current research hotspot. The methods mainly include biological method, stripping method, chemical precipitation method, etc. Although the acidity and alkalinity and temperature of these water bodies can be changed, the operating cost is very high. The adsorption method uses the physical properties between nitrogen and materials with large specific surface area or chemical affinity to remove nitrogen by adsorption, which has the advantages of less land occupation, simple method, no secondary pollution, reusable, and low cost. At present, there is still a lack of efficient nitrogen removal adsorbents, especially suitable for large-scale Applied Adsorbent Materials for Adsorbing Ammonia Nitrogen

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  • Preparation method and application of material for adsorption removal of organic matter and ammonia nitrogen

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Embodiment Construction

[0027] In order to make the technical means, creative features, goals and effects achieved by the present invention easy to understand, the present invention will be further described below in conjunction with specific embodiments.

[0028] Such as figure 1 As shown, this embodiment provides a method for preparing a material for adsorbing and removing organic matter and ammonia nitrogen, comprising the following steps:

[0029] 1) select clinoptilolite from natural zeolite and clean it, and wash it three times with distilled water;

[0030] 2) Stir in a high-speed mixer for 30min, then precipitate;

[0031] 3) Remove the upper turbid liquid with a 100 mesh screen;

[0032] 4) drying the cleaned zeolite in an oven at 100° C. for 24 hours;

[0033] 5) Put the dried zeolite into a muffle furnace for pre-activation, burn it at 450°C for 60 minutes, and cool it to room temperature to obtain material A, which is put into a sealed bag for later use;

[0034] 6) Prepare a 5mol / L s...

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Abstract

The invention discloses a preparation method of a material for adsorption removal of organic matter and ammonia nitrogen. The preparation method comprises the following steps that (1) clinoptilolite is selected from natural zeolite, cleaned and elutriated through distilled water for three times; (2) stirring is conducted for 30 min in a high-speed stirring machine, and then precipitation is conducted; (3) upper turbid liquid is removed through a sieve net of 100 meshes; (4) the cleaned clinoptilolite is dried for 24 h in a drying oven at 100 DEG C; (5) a material A is prepared; (6) a materialB is prepared; (7) a material C is prepared; (8) a material D is prepared; (9) a material E is prepared; (10) a material F is prepared; (11) a material G is prepared; (12) a material H is prepared; (13) a material I is prepared; (14) a material J is prepared; and (15) a final adsorption material K is prepared. The natural zeolite and coal ash which are low in cost and easy to obtain are taken as basic raw materials, the natural zeolite is modified by NaCl and then mixed with a 4A molecular sieve prepared from the coal ash according to a certain ratio, thus the novel adsorption material is obtained, and the material has a great organic matter and ammonia nitrogen adsorption effect.

Description

technical field [0001] The invention relates to a preparation method and application of a material for adsorbing and removing organic matter and ammonia nitrogen, and belongs to the technical field of sewage treatment. Background technique [0002] Water is a basic natural resource and a strategic economic resource. It occupies an important position in the national economy. High-quality clean water is the basis for human survival and development. Although my country has a large amount of water resources, the per capita water resources are equivalent to a quarter of the world's average level, and the water resources are seriously polluted, which puts forward urgent requirements for the control of water pollution and the improvement of water quality in our country. Therefore, how to reduce the concentration of ammonia nitrogen in non-drinking water sources in nature to the third type of surface water environmental standard, which is less than 1mg / l, is a current research hotsp...

Claims

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Application Information

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IPC IPC(8): B01J20/30C02F1/28C02F101/16C02F101/30
CPCB01J20/18C02F1/281C02F2101/16C02F2101/30
Inventor 王善鹏崔康平许为义刘彤
Owner ANHUI MEIZIRAN ENVIRONMENTAL TECH
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