Hydrogel flexible strain sensor with low Young modulus
A strain sensor, hydrogel flexible technology, applied in the direction of electromagnetic measurement device, electric/magnetic solid deformation measurement, etc., to achieve the effect of good strain-resistance sensitivity, high stretchability, excellent cutting resistance and compression deformation ability
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Embodiment 1
[0041] Prepare the following reagents in advance:
[0042] 1. Waterborne hexamethylene diisocyanate trimer (WHDT):
[0043] Feed 7g of ethylene glycol monomethyl ether (molecular weight 700) and hexamethylene diisocyanate trimer 5g (molecular weight 500), and mix and stir for 12 hours at 75°C to obtain water-based hexamethylene diisocyanate trimer (WHDT) .
[0044] 2. Ammonium persulfate solution:
[0045]0.04g initiator ammonium persulfate (APS) was dissolved in 50g water to obtain ammonium persulfate solution.
[0046] Preparation method of the strain sensor:
[0047] (1) Dissolve 7.1g of acrylamide monomer (AAm) and 0.02g of chemical cross-linking agent N,N-methylenebisacrylamide (MBAA) in ammonium persulfate (APS) solution, and ultrasonicate for 3 minutes to obtain Hydrogel mother liquor (preparation and use now);
[0048] (2) At room temperature, mix 5mL of the hydrogel mother liquor and 0.15g of the prepared chemical cross-linking agent WHDT, stir until the solution...
Embodiment 2
[0051] Prepare the following reagents in advance:
[0052] 1. Waterborne hexamethylene diisocyanate trimer (WHDT):
[0053] Feed 7g of ethylene glycol monomethyl ether (molecular weight 700) and hexamethylene diisocyanate trimer 5g (molecular weight 500), and mix and stir for 12 hours at 75°C to obtain water-based hexamethylene diisocyanate trimer (WHDT) .
[0054] 2. Ammonium persulfate solution:
[0055] 0.04g initiator ammonium persulfate (APS) was dissolved in water to obtain ammonium persulfate solution.
[0056] Preparation method of the strain sensor:
[0057] (1) Dissolve 7.1 g of acrylamide monomer (AAm) and 0.02 g of chemical cross-linking agent N, N-methylenebisacrylamide (MBAA) in ammonium persulfate solution, and ultrasonicate for 3 minutes to obtain a hydrogel Mother liquor (prepared and used now);
[0058] (2) At room temperature, mix 5mL of the hydrogel mother liquor and 0.24g of the chemical cross-linking agent WHDT, stir until the solution is clear; pour...
Embodiment 3~8
[0061] In Examples 3-8, the time for soaking the hydrogel in pyrrole and the initiator APS is shown in Table 1. All the other steps are as in Example 1.
[0062] Table 1 The soaking time of conductive hydrogel in pyrrole and APS
[0063]
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