Synthesis method and application of acrolein polymer
A technology of acrolein and polymer, which is applied in the application of acrolein polymer and the field of synthesizing acrolein polymer, which can solve the problems of uneven molecular weight of acrolein polymer, unsuitability for water purification and electronic packaging, and poor insulation. Achieve good bactericidal effect, reduce ammonia nitrogen and nitrite, and easily agglomerate
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Embodiment 1
[0018] A method for synthesizing an acrolein polymer, comprising the steps of:
[0019] S1. Distilling 150 kg of commercially available acrolein to obtain distilled acrolein; commercially available acrolein contains a polymerization inhibitor, which can be removed after distillation;
[0020] S2, adding the acrolein in S1 into the reaction kettle, and then adding 300 kg of solvent ethyl acetate;
[0021] S3. Dissolve 3 kilograms of catalyst azobisisobutyronitrile in 10 kilograms of ethyl acetate, then add it to the reaction kettle in S2, heat up to 61 ° C, react for 24 hours, and then cool down to 15 ° C to obtain a solution. Place in a filter press, pass through nitrogen pressure filtration, separate to obtain the mother liquor and filter cake, then place the mother liquor in the pressure filter again, pass through nitrogen pressure filtration, separate and obtain the filter cake, combine the filter cake obtained twice, and then add The filter cake was sprayed with 100 kg of...
Embodiment 2
[0024] A method for synthesizing an acrolein polymer, comprising the steps of:
[0025] S1. Distill 100 kg of commercially available acrolein to obtain distilled acrolein; commercially available acrolein contains a polymerization inhibitor, which can be removed after distillation;
[0026] S2, adding the acrolein in S1 into the reaction kettle, and then adding 300 kg of solvent ethyl acetate;
[0027] S3. Dissolve 3 kilograms of catalyst azobisisobutyronitrile in 4 kilograms of ethyl acetate, then add it to the reaction kettle in S2, heat up to 65 ° C, react for 24 hours, and then cool down to 15 ° C to obtain a solution. Place in a filter press, pass through nitrogen pressure filtration, separate to obtain the mother liquor and filter cake, then place the mother liquor in the pressure filter again, pass through nitrogen pressure filtration, separate and obtain the filter cake, combine the filter cake obtained twice, and then add The filter cake was sprayed with 100 kg of eth...
Embodiment 3
[0029] A method for synthesizing an acrolein polymer, comprising the steps of:
[0030] S1. Distill 120 kg of commercially available acrolein to obtain distilled acrolein; commercially available acrolein contains a polymerization inhibitor, which can be removed after distillation;
[0031] S2, adding the acrolein in S1 into the reaction kettle, and then adding 480 kg of solvent ethyl acetate;
[0032] S3. Dissolve 6 kilograms of catalyst azobisisobutyronitrile in 4 kilograms of ethyl acetate, then add it to the reaction kettle in S2, heat up to 70 ° C, react for 24 hours, and then cool down to 15 ° C to obtain a solution. Place in a filter press, pass through nitrogen pressure filtration, separate to obtain the mother liquor and filter cake, then place the mother liquor in the pressure filter again, pass through nitrogen pressure filtration, separate and obtain the filter cake, combine the filter cake obtained twice, and then add The filter cake was sprayed with 120 kg of eth...
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