Drilling fluid bionic lubricant, preparation method and applications thereof
A drilling fluid and lubricant technology, which is applied in the field of oilfield drilling fluids, can solve the problems of small adsorption amount on the surface of the mud cake on the well wall, affecting the lubrication effect, and difficult to firmly adsorb, and achieves easy mass production, easy preparation and environmental protection. Stable quality effect
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Embodiment 1
[0036]Add 20g polylysine (number average molecular weight 100kDa) to a 250mL three-neck flask with a thermometer and a mechanical stirrer, then add 150g deionized water to dissolve, and adjust the pH of the solution to 8.5 with sodium hydroxide. Then add 100g of methoxypolyethylene glycol-succinimide propionate (number average molecular weight 2kDa), stir and react at room temperature for 24h, then dry and pulverize the product solution at 120°C to obtain a bottle brush polymer PLL -g-PEG.
[0037] Add 100g of deionized water into a stirring flask at room temperature, add 2g of cetyl alcohol and 5g of bottle brush polymer PLL-g-PEG in sequence under stirring, and stir for 10 minutes to make the cetyl alcohol and the bottle Brush polymers are completely soluble in water. Then, 3 g of sodium alginate (100 kDa) was added into the reactor, and the biomimetic lubricant product A1 of the present invention was obtained after stirring for 1 hour.
Embodiment 2
[0039] Add 20g polylysine (number average molecular weight 100kDa) to a 250mL three-neck flask with a thermometer and a mechanical stirrer, then add 150g deionized water to dissolve, and adjust the pH of the solution to 8.5 with sodium hydroxide. Then add 150g of methoxy polyethylene glycol-succinimide propionate (number-average molecular weight 2kDa), stir and react at room temperature for 24h, then dry and pulverize the product solution at 120°C to obtain a bottle-brush polymer PLL -g-PEG.
[0040] Add 100g of deionized water into a stirring flask at room temperature, add 2g of cetyl alcohol and 5g of bottle brush polymer PLL-g-PEG in sequence under stirring, and stir for 10 minutes to make the cetyl alcohol and the bottle Brush polymers are completely soluble in water. Then, 3 g of sodium alginate (100 kDa) was added into the reactor, and the biomimetic lubricant product A2 of the present invention was obtained after stirring for 1 hour.
Embodiment 3
[0042] Add 20g polylysine (number average molecular weight 100kDa) to a 250mL three-neck flask with a thermometer and a mechanical stirrer, then add 150g deionized water to dissolve, and adjust the pH of the solution to 8.5 with sodium hydroxide. Then add 200g of methoxypolyethylene glycol-succinimide propionate (number average molecular weight 2kDa), stir and react at room temperature for 24h, then dry and pulverize the product solution at 120°C to obtain a bottle brush polymer PLL -g-PEG.
[0043] Add 100g of deionized water into a stirring flask at room temperature, add 3g of cetyl alcohol and 5g of bottle brush polymer successively under stirring, and stir for 10 minutes to make cetyl alcohol and bottle brush polymer completely Dissolve in water. Then, 3 g of sodium alginate (100 kDa) was added into the reactor, and the biomimetic lubricant product A3 of the present invention was obtained after stirring for 1 hour.
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