A kind of high damping 5083al/ti composite material and its preparation method
A technology of composite materials and titanium-based composite materials, which is applied in the field of high-damping 5083Al/Ti composite materials, can solve the problems that 5083Al/Ti composite materials have not yet been found, and achieve the effects of low price, improved damping performance and low density
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Embodiment 1
[0015] (1) Pure titanium powder with a particle size of 48 μm and NH with a particle size of 400 μm 4 HCO 3 The granules were weighed on a weighing balance according to the mass ratio of 3:1, and placed in a V-shaped mixer for 5 hours of rotation and mixing.
[0016] (2) Put the uniformly mixed powder in a square mold (length×width×height, 30mm×10mm×5mm), press it with a hydraulic press at room temperature, the pressure during pressing is 200MPa, and the holding time is 5 minutes , Place the pressed green body in a tube sintering furnace.
[0017] (3) Continuously feed argon with a purity of 99.9% into the tube-type sintering furnace as a protective gas, start heating the tube-type sintering furnace from room temperature, and raise the temperature to 200°C for 1.5 hours after 30 minutes. High-purity argon converts NH 4 HCO 3 CO produced by decomposition 2 and NH 3 Continuously discharge, then raise the temperature to 1050°C, keep the temperature for 1.5 hours, and then c...
Embodiment 2
[0020] (1) Pure titanium powder with a particle size of 48 μm and NH with a particle size of 500 μm 4 HCO 3 After the particles are weighed on a weighing balance according to the mass ratio of 17:3, they are placed in a V-type powder mixer and rotated for 5 hours.
[0021] (2) Put the uniformly mixed powder in a square mold (length×width×height, 30mm×10mm×5mm), press it with a hydraulic press at room temperature, the pressure during pressing is 100MPa, and the holding time is 5 minutes , Place the pressed green body in a tube sintering furnace.
[0022] (3) Continuously feed argon with a purity of 99.9% into the tube-type sintering furnace as a protective gas, heat the tube-type sintering furnace from room temperature, raise the temperature to 150°C for 2 hours after 30 minutes, and feed of high-purity argon to NH 4 HCO 3 CO produced by decomposition 2 and NH 3 Continuously discharge, then raise the temperature to 1050°C, keep it warm for 1 hour, and then cool down to ro...
Embodiment 3
[0025] (1) Pure titanium powder with a particle size of 48 μm and NH with a particle size of 300 μm 4 HCO 3 The particles were weighed on a weighing balance according to the mass ratio of 3:17, and placed in a V-type mixer for 5 hours of rotation and mixing.
[0026] (2) Put the uniformly mixed powder in a square mold (length×width×height, 30mm×10mm×5mm), press it with a hydraulic press at room temperature, the pressure during pressing is 300MPa, and the holding time is 5 minutes , Place the pressed green body in a tube sintering furnace.
[0027] (3) Continuously feed argon with a purity of 99.9% into the tube-type sintering furnace as a protective gas, heat the tube-type sintering furnace from room temperature, raise the temperature to 300°C for 1 hour after 30 minutes, and feed of high-purity argon to NH 4 HCO 3 CO produced by decomposition 2 and NH 3 Continuously discharge, then raise the temperature to 1050°C, keep the temperature for 2 hours, and then cool down to ...
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