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A support method for preventing sintering cracking of titanium-aluminum alloy liner compact

A drug-type cover, titanium-aluminum technology, applied in the direction of geometric CAD, etc., can solve the problems that affect the product processing size, cracking; if the support is too large, the inward shrinkage is difficult to proceed smoothly, etc., to improve the sintering quality of the compact efficiency, avoid sintering cracking, and reduce production costs

Active Publication Date: 2020-11-10
BEIJING INSTITUTE OF TECHNOLOGYGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, during the sintering process, the collapse and deformation of the compact will eventually lead to cracking, which affects the processing size of the product and reduces the pass rate of the product
[0003] The sum of the mass percentages of titanium powder and aluminum powder in the raw materials used for titanium-aluminum series alloys is greater than 70%. The sintering temperature of the alloy is 1300-1600°C, and the melting point of aluminum is 660°C, which makes aluminum occur during the sintering process. Melting, existing in the whole body in the form of liquid for a period of time, resulting in softening of the green body, if no support is used or the support is too small, the green body will collapse and deform under the influence of its own gravity. At the same time, Due to the friction between the bottom of the green body and the hearth, the inward shrinkage of the bottom of the green body is difficult to proceed smoothly during the sintering process, resulting in the asynchronous shrinkage of the bottom of the green body and the shrinkage of the top, resulting in cracks on the inner wall of the green body; Large, so that the green body after sintering is suspended on the support body, and the outer surface of the green body will be cracked under the influence of its own gravity

Method used

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  • A support method for preventing sintering cracking of titanium-aluminum alloy liner compact
  • A support method for preventing sintering cracking of titanium-aluminum alloy liner compact
  • A support method for preventing sintering cracking of titanium-aluminum alloy liner compact

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0094] (1) Determination of sintering shrinkage σ of titanium-aluminum alloy materials

[0095] Select the titanium-aluminum alloy material, wherein the mass percentage of titanium powder and aluminum powder is 75%, the mass percentage of niobium powder is 15%, and the mass percentage of tantalum powder is 10%, the powder after mixing The pressed compact is pressed into a compact with a pressure of 300MPa for 20 minutes, and processed into a standard size compact of Φ10×50mm; the pressed compact is placed in an atmosphere sintering furnace, and the process is carried out by using a process of 1500°C for 3 hours and argon protection atmosphere. Atmospheric pressure sintering; the size of the green body after sintering is measured to be Φ8.9×44.5mm, and the shrinkage rate σ in the longitudinal direction of this titanium-aluminum alloy material is 11% after calculation at 1500°C for 3 hours.

[0096] (2) Calculate the theoretical size of the titanium-aluminum alloy sintered bille...

Embodiment 2

[0107] (1) Determination of sintering shrinkage σ of titanium-aluminum alloy materials

[0108] Select the titanium-aluminum alloy material, wherein the mass percentage of titanium powder and aluminum powder is 70%, the mass percentage of zirconium powder is 20%, and the mass percentage of molybdenum powder is 10%, the powder after mixing The pressed compact is pressed into a compact with a pressure of 250MPa for 30 minutes, and processed into a standard size compact of Φ10×50mm; the compacted compact is placed in an atmosphere sintering furnace, and the process is carried out by using a process of holding at 1550°C for 4 hours and protecting the atmosphere with argon. Atmospheric pressure sintering; the size of the green body after sintering is measured to be Φ8.72×43.51mm, and the shrinkage rate σ in the longitudinal direction of this titanium-aluminum alloy material is 13% after calculation at 1550°C for 4 hours.

[0109] (2) Calculate the theoretical size of the titanium-a...

Embodiment 3

[0119] (1) Determination of sintering shrinkage σ of titanium-aluminum alloy materials

[0120] Select the titanium-aluminum series alloy material, wherein the mass percentage of titanium powder and aluminum powder is 80%, the mass percentage of tantalum powder is 15%, and the mass percentage of molybdenum powder is 5%, the powder after mixing The pressed compact is pressed into a green compact with a pressure of 280MPa for 30 minutes, and processed into a standard size green compact of Φ10×50mm; the pressed green compact is placed in an atmosphere sintering furnace, and the process is carried out by using a process of 1600°C for 4 hours and argon protection atmosphere. Atmospheric pressure sintering; the size of the green body after sintering is measured as Φ8.86×44.27mm, and the shrinkage rate σ in the longitudinal direction of this titanium-aluminum alloy material is 11.5% under the condition of 1600 ° C for 4 hours.

[0121] (2) Calculate the theoretical size of the titani...

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Abstract

The invention provides a supporting method for preventing sintered cracking of a shaped charge cover pressed blank of a titanium and aluminum serial alloy and belongs to the technical field of sintering control. By calculating the sintering shrinkage rate of a titanium and aluminum serial alloy material, a rigid supporting body structure can be designed reasonably, the dimension of the obtained rigid supporting body is consistent to a theoretical inner dimension of an obtained sintered blank after the shaped charge cover pressed blank is sintered, the shaped charge cover pressed blank can be supported sufficiently, cracking due to excessive deformation of the shaped charge cover pressed blank in the sintering process as a result of gravity and sintered cracking due to softening and collapsing are avoided, and the pressed blank sintering percent of pass is improved obviously. An inward pressure can be applied to the shaped charge cover pressed blank by burying sand, so that the bottom of the pressed blank can be promoted to shrink inward in the sintering process so as to further inhibit cracks as a result of non-synchronous sintering and shrinking in the pressed blank. Embodiments verify that the method can prevent sintered cracking of the shaped charge cover pressed blank of the titanium and aluminum serial alloy, and the sintering percent of pass of the pressed blank can reachover 99%.

Description

technical field [0001] The invention relates to the technical field of sintering control, in particular to a support method for preventing sintering cracking of a titanium-aluminum alloy liner mold compact. Background technique [0002] Petroleum perforating charge is a device used to break through the concrete and rock between the casing and the production layer to provide circulation channels for oil and gas. At present, most petroleum perforating bullets use a shaped charge structure, and the liner is a key component of the shaped charge structure. The production quality of the liner directly determines the effect of the perforating charge. The traditional drug-type cover is usually prepared by melting casting and hot isostatic pressing sintering. Low efficiency also increases production cost. Therefore, powder metallurgy near-net forming method is now mostly used to prepare thin-walled hollow conical parts of titanium-aluminum alloys. The method includes cold isostati...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F5/00B22F3/02B22F3/10G06F30/17
CPCB22F3/02B22F3/1007B22F5/00
Inventor 刘金旭徐菡卿蔡奇贺川冯新娅李树奎吕延伟
Owner BEIJING INSTITUTE OF TECHNOLOGYGY