Transposition method of acetophenone isomer
A technology of isomers and acetophenone, which is applied in the field of transposition of acetophenone isomers, can solve the problems of m-dichlorobenzene, such as high price, high specific gravity, and high production cost, and achieve high transposition efficiency, The effect of reducing resource waste and stabilizing performance
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Embodiment 1
[0023] A kind of transposition method of acetophenone isomer
[0024] Including the following steps:
[0025] Step I, 2,4-dichloroacetophenone synthesis: select m-dichlorobenzene and acetyl chloride raw materials, react to obtain 2,4-dichloroacetophenone crude product; 2,4-dichloroacetophenone crude product, 2 , the content of 4-dichloroacetophenone is 92.5%; the content of 2,6-dichloroacetophenone is 5%;
[0026] Step II, transposition reaction: Add the crude product of 2,4-dichloroacetophenone obtained in step I into cyclohexane with a purity of 99.0%, and then add sulfuric acid with a mass fraction of 98%. Under the condition of reaction for 3 hours, the transposition is completed; wherein, the mass ratio of crude 2,4-dichloroacetophenone, cyclohexane with a purity of 99.0% and sulfuric acid with a mass fraction of 98% is 100:300:11.5.
[0027] In the above, the transposition process of the transposition reaction is:
[0028] In the above, after the transposition is co...
Embodiment 2
[0030] A kind of transposition method of acetophenone isomer
[0031] Including the following steps:
[0032] Step I, 2,4-dichloroacetophenone synthesis: select m-dichlorobenzene and acetyl chloride raw materials, react to obtain 2,4-dichloroacetophenone crude product; 2,4-dichloroacetophenone crude product, 2 , the content of 4-dichloroacetophenone is 94.0%; the content of 2,6-dichloroacetophenone is 5%;
[0033] Step II, transposition reaction: Add the crude product of 2,4-dichloroacetophenone obtained in Step I into cyclohexane with a purity of 99.0%, and then add sulfuric acid with a mass fraction of 98%. The transposition was completed by reacting under the conditions for 5 hours; wherein, the mass ratio of crude 2,4-dichloroacetophenone, cyclohexane with a purity of 99.0% and sulfuric acid with a mass fraction of 98% was 100:300:12.5.
[0034] In the above, the transposition process of the transposition reaction is:
[0035] In the above, after the transposition is ...
Embodiment 3
[0037] A kind of transposition method of acetophenone isomer
[0038] Including the following steps:
[0039] Step I, 2,4-dichloroacetophenone synthesis: select m-dichlorobenzene and acetyl chloride raw materials, react to obtain 2,4-dichloroacetophenone crude product; 2,4-dichloroacetophenone crude product, 2 , the content of 4-dichloroacetophenone is 93.0%; the content of 2,6-dichloroacetophenone is 5%;
[0040] Step II, transposition reaction: Add the crude product of 2,4-dichloroacetophenone obtained in step I into cyclohexane with a purity of 99.0%, and then add sulfuric acid with a mass fraction of 98%, at a temperature of 79°C The reaction was carried out under the conditions for 3.5 hours to complete the transposition; wherein, the mass ratio of crude 2,4-dichloroacetophenone, cyclohexane with a purity of 99.0% and sulfuric acid with a mass fraction of 98% was 100:300:11.8.
[0041] In the above, the transposition process of the transposition reaction is:
[0042]...
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