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Preparation method of anti-radiation silicon oxide anti-reflection film

A technology of silicon oxide and anti-reflection coating, applied in coatings and other directions, can solve the problems of weakened performance, affecting the efficiency of space solar cells, and failure to achieve protection, etc., and achieve the effect of simple operation, increased practicability, hardness and controllability

Inactive Publication Date: 2020-06-23
YUNNAN NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Anti-reflection coating, also known as anti-reflection coating, its main function is to reduce or eliminate the reflected light from optical surfaces such as lenses, prisms, and plane mirrors, thereby increasing the light transmission of these components, reducing or eliminating stray light in the system, anti-reflection coating Applications in space are inevitably affected by rays and high-energy particles in space, resulting in weakened performance, which greatly affects the efficiency of space solar cells, and cannot protect space X-rays, γ-rays and neutrons to a certain extent: Therefore, there is a need for a preparation method of radiation-resistant silicon oxide anti-reflection film

Method used

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Embodiment 1

[0019] A preparation method of anti-irradiation silicon oxide anti-reflective film, including configuring initial alkaline SiO 2 Sol coating solution, adding emulsifier polytetrafluoroethylene and nano-level powdered lead chloride, preparing a film on the surface of the substrate and then supercritically drying it to form a certain aerogel structure and film heat treatment, the preparation method is as follows ;

[0020] The preparation steps are as follows:

[0021] Step 1: Configure initial alkaline SiO 2 Sol coating solution: mix and stir ethyl orthosilicate (TEOS) and absolute ethanol (EtOH). After the solution is evenly stirred, slowly add a mixed solution of absolute ethanol, deionized water, and ammonia water, stir and mix evenly and then stand still Home aging

[0022] Step 2: Add the emulsifier polytetrafluoroethylene emulsion, after the solution is stabilized by aging, add a certain amount of nano-powder lead chloride into it, seal and stir to make the lead chloride unifor...

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Abstract

The invention discloses a preparation method of an anti-radiation silicon oxide anti-reflection film. The preparation method is characterized by comprising the following steps: preparing an initial alkaline sol coating solution, adding an emulsifier polytetrafluoroethylene and nano-scale lead chloride powder, preparing a film on the surface of a substrate, carrying out supercritical drying to forma certain aerogel structure, carrying out a film heat treatment, preparing an initial alkaline sol coating solution; mixing and stirring tetraethoxysilane and anhydrous ethanol, slowly dropwise adding a mixed solution of anhydrous ethanol, deionized water and ammonia water after the solution is stirred uniformly, stirring and mixing uniformly, standing, aging, adding an emulsifier polytetrafluoroethylene emulsion, adding a certain amount of nano-powder lead chloride into the solution after the solution is aged and stabilized, sealing and stirring. The preparation method has the advantages that the operation is simple, the technological process is simplified, the prepared silicon oxide anti-reflection film can be accurately controlled to effectively protect space rays, the hardness is highand controllable, the silicon oxide anti-reflection film is suitable for space solar cells, and the practicability is high.

Description

Technical field [0001] The invention relates to the technical field of anti-reflection films, in particular to a method for preparing radiation-resistant silicon oxide anti-reflection films. Background technique [0002] Anti-reflection coating, also known as anti-reflection coating, its main function is to reduce or eliminate the reflected light of optical surfaces such as lenses, prisms, and plane mirrors, thereby increasing the amount of light transmitted by these components, reducing or eliminating stray light in the system, and anti-reflection coating The application in space is inevitably affected by the rays and high-energy particles in the space, resulting in weakening of its performance, which greatly affects the efficiency of space solar cells, and cannot protect space X-rays, gamma rays and neutrons to a certain extent: Therefore, there is a greater need for a method for preparing radiation-resistant silicon oxide anti-reflection film. Summary of the invention [0003]...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C17/32
CPCC03C17/009C03C2217/732C03C2218/32C03C2218/111C03C2218/116C03C2218/112C03C2218/118
Inventor 涂洁磊孙晓宇李雷张炜楠胡凯
Owner YUNNAN NORMAL UNIV