Anti-tumor drug carrier, preparation method thereof and pharmaceutical preparation containing anti-tumor drug carrier
A technology for anti-tumor drugs and pharmaceutical preparations, applied in the directions of anti-tumor drugs, medical preparations containing active ingredients, drug combinations, etc. Problems such as low yield of micro-particles, to achieve the effect of high uniformity, small particle size and good permeability
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Embodiment 1
[0036] Example 1: Different doses 60 Effect of CO irradiation on the release of tumor cell vesicles
[0037] Experimental materials:
[0038] Lung cancer cells NCI-H292, intestinal cancer cells HCT-116, leukemia cell HL60 three cell lines were purchased from China Typical Savings Center.
[0039] 60 The Co radiation source is a TIL type 60CO treatment machine.
[0040] Nanosight NS300 Granules Tracking Analyzer: Malvin, United Kingdom.
[0041] Flow cytometry: BD FACSCANTO II flow cytometer.
[0042] Raw materials were purchased from Dalian Meilun Biotechnology Co., Ltd., Cisplatin CAS: 15663-27-1; Methadate CAS: 59-05-2; Hydrochloride CAS: 25316-40-9.
[0043] The apoptosis dyeing kit is a Biolegend Annexin V-FITC / PI apoptosis test kit.
[0044] 2. Experimental steps
[0045]Take three tumor cells (lung cancer NCI-H292, intestinal cancer HCT-116, leukemia cell HL60), each cell number is 1 × 10 8 / Dish. The three cells were used for GIBCO RPMI-1640 medium, and 10% of the four s...
Embodiment 2
[0053] Example 2: Comparison of the number and particle diameter of the cell vesicles produced by γ-ray irradiation and UVB irradiation
[0054] Experimental material
[0055] Lung cancer cell NCI-H292, intestinal cancer cell HCT-116, leukemia cell HL60 three cell lines were purchased from China Typical Savings Center CCTCC;
[0056] 60 CO radiation source is a TIL type 60CO treatment machine;
[0057] UVB ultraviolet lamps are Philips UVB 311NM TL 100W / 01 ultraviolet lamp;
[0058] Nanosight NS300 Granules Tracking Analyzer: Malvin, United Kingdom;
[0059] Flow cytometry: BD FACSCANTO II flow cytometry;
[0060] Raw materials were purchased from Dalian Meilun Biotechnology Co., Ltd., Cisplatin CAS: 15663-27-1; Methadate CAS: 59-05-2; Hydrochloride CAS: 25316-40-9.
[0061] 2. Experimental steps
[0062] Gamma ray irradiation group: three cells in Example 1 60 The vesicle production after Co ray irradiation, selects a preferred preparation conditions: 10 Gy irradiation, dose ra...
Embodiment 3
[0067] Example 3 Comparison of pharmaceutical vesicles produced under two preparation conditions on in vitro killing effects of tumor cells
[0068] Experimental material
[0069] Drugs: Raw materials were purchased from Dalian Meilun Biotechnology Co., Ltd., hydrochloride CAS: 25316-40-9.
[0070] Lung cancer cells NCI-H292, intestinal cancer cells HCT-116, leukemia cell HL60 three cell lines were purchased from China Typical Savings Center.
[0071] 60 The Co radiation source is a TIL type 60CO treatment machine.
[0072] UVB ultraviolet lamps for Philips UVB 311NM TL 100W / 01 UV lamp tube
[0073]Nanosight NS300 Granules Tracking Analyzer: Malvin, United Kingdom.
[0074] The apoptosis dyeing kit is a Biolegend Annexin V-FITC / PI apoptosis test kit.
[0075] 2. Experimental steps
[0076] According to the steps of the two preparation methods in Example 2, a polyxin vesicles of three tumor cell sources were prepared by gamma rays and UVB, and the Nanosight NS300 was counted, a...
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