Novel energy storage material for improving heat and mass transfer efficiency
A technology of energy storage materials and phase change materials, which is applied in the field of phase change energy storage, can solve the problems of large decrease in latent heat of phase change, low heat and mass transfer efficiency of energy storage materials, and affecting the thermal conductivity of phase change materials.
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[0027] (1) Modification of graphene oxide: 200mg graphene oxide (Beijing Deke Daojin Technology Co., Ltd., synthesized by the Hummers method) was mixed with 100mL deionized water, and ultrasonic 2h was formed to form a uniform graphene oxide dispersion; Under stirring conditions, mix absolute ethanol-toluene (volume ratio 1:1) containing 400 mg of silane coupling agent γ-phthalimidopropyltrimethoxysilane (CAS: 154717-09-6) The solution was added dropwise into the graphene oxide dispersion; after the dropwise addition, the pH was adjusted to 5.0 with acetic acid. Then react at 70° C. for 24 h, cool to room temperature, centrifuge, and wash the precipitate three times with absolute ethanol and deionized water to remove unreacted silane coupling agent. Vacuum drying to obtain modified graphene oxide powder.
[0028] FT-IR spectra showed that the modified graphene oxide powder increased by 2960 cm compared with unmodified graphene oxide -1 (CH 3 ), 2890cm -1 (CH 2 ), 1740cm ...
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