Heat-resistant ethylene-vinyl acetate rubber cable material and preparation method thereof
A technology of vinyl acetate and cable materials, which is applied to rubber insulators, organic insulators, etc., and can solve problems such as insufficient development efforts and insufficient selection of special materials
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[0030] The invention discloses a preparation method of ethylene-vinyl acetate rubber heat-resistant cable material. The preparation method comprises the following steps:
[0031] Step 1, add each component in turn according to the formula amount, and disperse evenly under closed mixing conditions supplemented by ultrasonic and microwave conditions to obtain mixture A;
[0032] Step 2, adding the crosslinking agent to the mixture A under open mixing conditions supplemented by ultrasonic and microwave conditions, kneading evenly and rolling to obtain the mixture B;
[0033] Step 3: Extrude, vulcanize and cross-link the mixture B under extrusion vulcanization conditions supplemented by ultrasonic and microwave conditions, to obtain the ethylene-vinyl acetate rubber heat-resistant cable material.
[0034] Preferably, the order of adding the components in step 1 is: sequentially add filler reinforcing agent, crosslinking aid, plasticizer, anti-aging agent, colorant, processing aid,...
Embodiment 1
[0057] Embodiment 1: This embodiment provides a kind of preparation method of ethylene-vinyl acetate rubber heat-resistant cable material, and its preparation method comprises the following steps:
[0058] Step 1, 25kg calcined kaolin, 1.2kg triallyl isocyanate TAIC, 4kg trioctyl trimellitate (TOTM), 0.5kg tetrakis[β-(3,5-di-tert-butyl-4 -Hydroxyphenyl) propionic acid] pentaerythritol ester (1010), 0.5kg 2,2,4-trimethyl-1,2-dihydroquinoline polymer (RD), 0.08kg blue toner, 3kg magnesium oxide, 1.5kg of zinc calcium stearate, 3kg of ethylene-propylene rubber (EPDM7001), and 32kg of ethylene-vinyl acetate rubber (EVM) were sequentially added to the closed rubber mixer, supplemented by a microwave with a power of 200W, and the power was 200W, the frequency The ultrasonic wave is 40kHz, and the ultrasonic wave is intermittently stopped for 20s every 10s. Under the conditions of 70°C and 40r / min, after banburying for 8min, the temperature is raised to 80°C, banburying for 40min, an...
Embodiment 2
[0067] Embodiment 2: This embodiment provides a kind of preparation method of ethylene-vinyl acetate rubber heat-resistant cable material, and its preparation method comprises the following steps:
[0068] Step 1, 25kg calcined kaolin, 1.2kg triallyl isocyanate TAIC, 4kg trioctyl trimellitate (TOTM), 0.5kg tetrakis[β-(3,5-di-tert-butyl-4 -Hydroxyphenyl) propionic acid] pentaerythritol ester (1010), 0.5kg 2,2,4-trimethyl-1,2-dihydroquinoline polymer (RD), 0.06kg red toner, 0.01kg carbon black N660, 3kg of magnesium oxide, 1.5kg of zinc calcium stearate, 3kg of ethylene-propylene rubber (EPDM7001), and 32kg of ethylene-vinyl acetate rubber (EVM) were sequentially added to the closed rubber mixer, supplemented by a microwave with a power of 200W, And the ultrasonic power is 100W, the frequency is 60kHz, and the ultrasonic wave is intermittently stopped for 20s every 10s. Under the condition of 90°C and the speed of 40r / min, after banburying for 10min, the temperature is raised to...
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Abstract
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