Quartz crystal microbalance sensor, preparation method and application thereof
A technology of quartz crystal and microbalance, which is applied in the field of sensor detection, can solve the problems of shortened life and the influence of the electrode detection performance of QCM crystal oscillator, and achieve the effects of prolonging service life, good piezoelectric effect and good response relationship
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[0034] Specifically, the preparation method of the quartz crystal microbalance sensor comprises the following steps:
[0035] Step 1, take by weighing the Zn(CH 3 COO) 2 2H 2 O and HO(CH 2 ) 2 NH 2 and dissolved in an equal amount of C 4 h 10 o 2 in, stir evenly to obtain HO(CH 2 ) 2 NH 2 solution with Zn(CH 3 COO) 2 2H 2 O solution;
[0036] Step 2, the Zn(CH 3 COO) 2 2H 2 O solution was slowly added to HO(CH 2 ) 2 NH 2 solution, stir evenly to obtain ZnO gel; then add polyethylene glycol to obtain ZnO solution, and static aging for later use;
[0037] Step 3, immerse the electrode of the crystal oscillator into the ZnO solution prepared in step 2 and take it out, repeat 2-3 times, dry, and anneal to obtain an electrode coated with ZnO seeds;
[0038] Step 4. Configure ZnNO 3 , (CH 2 ) 6 N 4 , a mixed solution of β-cyclodextrin, the electrode coated with ZnO seeds is immersed in the mixed solution to prepare an electrode coated with a ZnO nanocomposit...
Embodiment 1
[0047] A kind of quartz crystal microbalance sensor is provided in the present embodiment, it comprises: crystal oscillator, the electrode surface of this crystal oscillator is decorated with self-cleaning coating, and this self-cleaning coating is ZnO / TiO 2 nanocomposite film.
[0048] The preparation method of this quartz crystal microbalance sensor comprises the steps:
[0049] Step 1, weigh 0.05mol Zn(CH 3 COO) 2 2H 2 O and 0.05mol HO(CH 2 ) 2 NH 2 and dissolved in 50ulC 4 h 10 o 2 in, stir evenly to obtain HO(CH 2 ) 2 NH 2 solution with Zn(CH 3 COO) 2 2H 2 O solution; wherein, the stirring temperature is 60°C, and the stirring time is 30min;
[0050] Step 2, the Zn(CH 3 COO) 2 2H 2 O solution was slowly added to HO(CH 2 ) 2 NH 2 In the solution, stir evenly to obtain ZnO gel; then add 0.3g polyethylene glycol-400 to obtain ZnO solution, and static aging for later use; wherein, the stirring temperature is 60°C, the stirring time is 2h, and the static a...
Embodiment 2
[0056] The difference with the above-mentioned embodiment is that:
[0057] The preparation method of the quartz crystal microbalance sensor provided in this embodiment comprises the following steps:
[0058] Step 1, weigh 0.1mol Zn(CH 3 COO) 2 2H 2 O and 0.1mol HO(CH 2 ) 2 NH 2 and dissolved in 50ulC 4 h 10 o 2 in, stir evenly to obtain HO(CH 2 ) 2 NH 2 solution with Zn(CH 3 COO) 2 2H 2 O solution; wherein, the stirring temperature is 60°C, and the stirring time is 30min;
[0059] Step 2, the Zn(CH 3 COO) 2 2H 2 O solution was slowly added to HO(CH 2 ) 2 NH 2 In the solution, stir evenly to obtain a ZnO gel; then add 0.6g polyethylene glycol-400 to obtain a ZnO solution, which is statically aged for use; wherein, the stirring temperature is 60°C, the stirring time is 2h, and the static aging time is 24h;
[0060] Step 3. Immerse the electrode of the crystal oscillator into the ZnO solution prepared in step 2 and take it out, repeat 2-3 times, dry, the im...
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