MoS2/CeO2 composite gas-sensitive material as well as preparation method and application thereof
A gas-sensitive material, mos2 technology, applied in the analysis of materials, material resistance, material analysis by electromagnetic means, etc., can solve the problems of high working temperature, high resistance of pure cerium oxide, etc., to achieve good selectivity and good reversibility , fast response/recovery effect
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Embodiment 1
[0049] Such as Figure 1-11 As shown, a MoS 2 / CeO 2 Composite gas sensing material, by adding CeO 2 Nanoparticles tightly attached to MoS 2 The surface of nanoflowers to get MoS 2 / CeO 2 Composite gas sensing material, the MoS 2 Flower-like structure with many worm-like micelles.
[0050] The MoS 2 The nanoflowers have a diameter of 600-720nm and a thickness of 200-240nm, and the CeO 2 The diameter of the nanoparticles is 10-30nm.
[0051] The present invention also includes a method for preparing MoS 2 / CeO 2 Composite gas-sensitive material method,
[0052] ① Preparation of MoS 2 Hydrothermal solution: under strong magnetic stirring, Na 2 MoO 4 2H 2 O and thioacetamide are added to deionized water to obtain a mixed solution, and 2mol / L of HCl is added to the mixed solution until the pH value of the solution reaches 5;
[0053] ② Preparation of MoS 2 Powder: Move the mixture obtained in step ① into a reaction kettle, heat at 220°C for 14 hours, and wash with...
Embodiment 2
[0078] The present invention also includes a method for preparing MoS 2 / CeO 2 Composite gas-sensitive material method,
[0079] ① Preparation of MoS 2 Hydrothermal solution: 1.0g of Na 2 MoO 4 2H 2 O and 1.2g of thioacetamide were added to 80mL of deionized water, the stirring temperature was controlled at 40-50°C, the stirring speed was 600-800rpm, and the stirring time was 10-15min, and 2mol / L of HCl was added to adjust the pH of the solution to 5 to obtain MoS 2 hydrothermal solution;
[0080] ② Preparation of MoS 2 Powder: Move the mixture obtained in step ① into a reaction kettle, heat at 220°C for 14 hours, and wash with deionized water several times to obtain MoS 2 Powder, and dry, the drying temperature is 60-80°C, and the drying time is 12-24h;
[0081] ③The MoS obtained in step ② 2 Added to 50mL of deionized water and 30mL of ethanol mixed solution, then, by fully stirring the Ce(NO 3 ) 3 ·6H 2 O is added and dissolved;
[0082] ④ Move the dispersion o...
Embodiment 3
[0086] A gas-sensitive coating for MoS 2 / CeO 2 The preparation method of the ethanol gas sensor of composite material is carried out according to the following steps:
[0087] ① First, 1.0g of Na 2 MoO 4 2H 2 O and 1.2 g of thioacetamide were added to 80 mL of deionized water to obtain a mixed solution, which was magnetically stirred at a speed of 600 rpm for 10 min. Next, add 2mol / L HCl into the mixture solution until the pH value of the solution reaches 5;
[0088] ② Transfer the mixture obtained in step ① to a 100mL reactor, and heat at 220°C for 14h. MoS was obtained after several washes with deionized water 2 Powder, dried at 60°C for 12h;
[0089] ③Add 0.5g of MoS obtained in step ② 2 Add to 50 mL of deionized water and 30 mL of ethanol. Then, 0.06 g of Ce(NO 3 ) 3 ·6H 2 O is dissolved in the above dispersion, and the molar ratio of Ce to Mo is 1:20;
[0090] ④ Transfer the dispersion obtained in step ③ to a 100mL reactor, and treat it at 180°C for 24h. Th...
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