Sweet-scented osmanthus extract, preparation method thereof and cosmetics
A technology of osmanthus fragrans extract and osmanthus fragrans, which is applied to cosmetics, cosmetic preparations, cosmetic preparations and other directions, can solve the problems of poor stability of active ingredients, reduced efficacy, deepening color and the like, and achieves high content of active ingredients, rapid and effective extraction, The effect of low cost of raw materials
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[0047] According to a first aspect of the present invention, a kind of preparation method of osmanthus fragrans extract is provided, comprising the following steps:
[0048] (a) mixing the pretreated osmanthus fragrans with a solvent and carrying out negative pressure extraction to obtain an extract;
[0049] The extract is subjected to solid-liquid separation to obtain a supernatant;
[0050] (b) Concentrating the supernatant and using an adsorption resin for adsorption, and then eluting to obtain an eluent;
[0051] The eluate is concentrated and freeze-dried to obtain the osmanthus extract containing verbascoside and salidroside.
[0052] Specifically, the pretreatment in step (a) of the present invention is to prepare the fresh osmanthus into a form suitable for extraction. Typical but non-limiting pretreatment steps may be, for example, drying and / or powdering.
[0053] Negative pressure extraction refers to the use of vacuum decompression during extraction, so that the...
Embodiment 1
[0097] The present embodiment provides a kind of preparation method of sweet-scented osmanthus extract, and technological process diagram is as follows figure 1 shown, including the following steps:
[0098](a) after drying, 1 kg of dried sweet-scented osmanthus obtained is mechanically pulverized, mixed with a solvent and subjected to negative pressure extraction to obtain an extract; wherein, the solvent is water, and the solid-liquid ratio of sweet osmanthus and solvent is 1:20, and the pressure of negative pressure extraction is -0.06MPa, the temperature of negative pressure extraction is 30°C, the time of negative pressure extraction is 60min, and the number of negative pressure extraction is 1 time;
[0099] centrifuging the extract to remove the precipitate to obtain a supernatant; the centrifugation speed is 3000r / min;
[0100] (b) after concentrating the supernatant, use D101 macroporous adsorption resin to adsorb, and then use water and 30% ethanol aqueous solution ...
Embodiment 2
[0103] This example provides a preparation method of sweet-scented osmanthus extract, except that the temperature of negative pressure extraction in step (a) is 40° C., other steps are the same as in Example 1.
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