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Sampling device and sampling method for ultralow-concentration tobacco flavor substances

An aroma substance and ultra-low concentration technology, which is applied to the field of sampling devices for ultra-low concentration tobacco aroma substances, can solve the problems of accelerating the adsorption speed of tobacco natural aroma substances, unable to judge that the aromatization equipment is completely purified, and the detection sensitivity of GC-MS is reduced. , to facilitate independent filling and disassembly sampling, improve detection accuracy, and facilitate subsequent detection.

Pending Publication Date: 2022-06-28
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In the prior art, the Chinese patent with the publication number CN203737062U discloses a device for extracting the aroma and fragrance of tobacco in the waste gas of the cone-barrel tobacco leaf processing. Accelerate the adsorption speed of tobacco flavor and fragrance in the waste gas, and have a high recovery rate of fragrance, and at the same time speed up the speed of waste gas passing through the fragrance collection device, and improve production efficiency; its eluting device circulates and cleans the absorbent in the fragrance absorption layer, The elution speed can be greatly accelerated. On the one hand, the patent does not remove the interfering impurities in a targeted manner, which will reduce the detection accuracy of subsequent aroma substances. If the ultra-low concentration of fragrance substances are collected and tested together, there will be interference between them, resulting in a decrease in the sensitivity of subsequent GC-MS detection, so it is impossible to judge whether the fragrance adding equipment is completely purified

Method used

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  • Sampling device and sampling method for ultralow-concentration tobacco flavor substances
  • Sampling device and sampling method for ultralow-concentration tobacco flavor substances
  • Sampling device and sampling method for ultralow-concentration tobacco flavor substances

Examples

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Effect test

Embodiment 1

[0044] like figure 1 As shown, a sampling device for ultra-low concentration tobacco aroma substances includes a pretreatment system 1, a gas concentration system 2, and an inflator 3 that are communicated in sequence, and the pretreatment system 1 includes a heating device 11 communicated in sequence, a first communicated Pipe 12, gas impurity removal device 13, the gas concentration system 2 includes a second communication pipe 21, a first sampling pipe 22 filled with polar adsorbent, a second sampling pipe 23 filled with non-polar adsorbent, Three communication pipes 24, the first sampling pipe 22 and the second sampling pipe 23 are detachably connected in parallel between the second communication pipe 21 and the third communication pipe 24, and the second communication pipe 21 includes a A first outlet 212 of the gas flow check valve 211, a second outlet 214 of the second gas flow check valve 213, the third communication pipe 24 is provided with a first inlet 242 of the fi...

Embodiment 2

[0049] like figure 1 As shown, a sampling device for ultra-low concentration tobacco aroma substances includes a pretreatment system 1, a gas concentration system 2, and an inflator 3 that are communicated in sequence, and the pretreatment system 1 includes a heating device 11 communicated in sequence, a first communicated Pipe 12, gas impurity removal device 13, the gas concentration system 2 includes a second communication pipe 21, a first sampling pipe 22 filled with polar adsorbent, a second sampling pipe 23 filled with non-polar adsorbent, Three communication pipes 24, the first sampling pipe 22 and the second sampling pipe 23 are detachably connected in parallel between the second communication pipe 21 and the third communication pipe 24, and the second communication pipe 21 includes a A first outlet 212 of the gas flow check valve 211, a second outlet 214 of the second gas flow check valve 213, the third communication pipe 24 is provided with a first inlet 242 of the fi...

Embodiment 3

[0065] A method for sampling ultra-low concentration tobacco aroma substances using a sampling device for ultra-low concentration tobacco aroma substances as shown in Example 2, the difference is that the surface area of ​​the tobacco straw hydrothermal charcoal described in step S1 is 1000g / m2 2 , the aperture is 2nm, the heating device 11 is heated at 50°C for 60min in step S2, in step S3, the time of normal temperature operation is 10min, the gas flow rate controlled by the first gas flow one-way control valve 211 is 0, in step S5, heating and desorption The temperature is 80 ℃, and the ultra-low concentration tobacco flavor substance to be tested is obtained.

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Abstract

The invention discloses a sampling device and a sampling method for ultralow-concentration tobacco flavor substances, and the sampling device comprises a pretreatment system, a gas concentration system and an inflation device which are communicated in sequence, the gas concentration system comprises a second communicating pipe, a first sampling pipe filled with a polar adsorbent, a second sampling pipe filled with a non-polar adsorbent and a third communicating pipe, the first sampling pipe and the second sampling pipe are detachably connected between the second communicating pipe and the third communicating pipe in parallel, and a first circulating pipe and a second circulating pipe are further arranged; the special adsorbent filled is controlled through opening and closing of the valve, residual aroma substances of the added cigarette shreds are subjected to impurity removal, then the special adsorbent is adopted for cyclic enrichment according to polarity classification, enrichment is thorough, no residues exist, mutual interference among complex aroma substance components is reduced, the sensitivity of the components in the subsequent detection process is improved, and the detection accuracy is improved. Whether the perfuming equipment is completely purified or not can be conveniently judged.

Description

technical field [0001] The invention relates to the field of tobacco manufacturing, in particular to a sampling device for ultra-low concentration tobacco flavor substances and a sampling method thereof. [0002] technical background [0003] The tobacco industry is an important part of the national economic system. Flavoring of cut tobacco is an indispensable key process in the tobacco manufacturing process. of tobacco. With the continuous improvement of the automation control level of the tobacco silk production line, the requirements for the quality of silk and flavoring production are more stringent. When producing different brands of tobacco, it is necessary to deeply purify the flavoring equipment to remove the residual flavor, so as to avoid the smell of different brands of cut tobacco and ensure the efficient operation of the production line. However, at present, judging whether the aromatherapy equipment has completed deep purification mainly relies on the judgment...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/22G01N1/24G01N1/34G01N1/40G01N1/44
CPCG01N1/2214G01N1/24G01N1/34G01N1/405G01N1/44
Inventor 李冉叶明樵罗民刘辉王波周萍芳张风光赵磊张亮
Owner HUBEI CHINA TOBACCO IND
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