Preparation method of superlattice ceramic atomizing core
A superlattice and atomizing core technology, applied in the field of atomization, can solve the problems of easy oxidation and short service life of the atomizing core, and achieve the effects of prolonging the service life, promoting uniform distribution and improving thermal efficiency.
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[0025] In order to further understand the contents of the present invention, the present invention will be described in detail in conjunction with examples. A method for preparing a superlattice ceramic atomizing core of the present invention is characterized in that it comprises the following steps:
[0026] Step 1: Prepare a nano-superlattice electrothermal film treatment solution, and put the prepared electrothermal film treatment solution into the coating solution storage bin of the vacuum plasma sputtering coating machine;
[0027] Step 2: Pass the ceramic substrate to the feeding and retrieving manipulator through the feeding and feeding machine, send it into the high-temperature vacuum plasma coating machine, start the sputtering coating machine, and obtain an electrothermal film on the surface of the ceramic substrate;
[0028] Step 3: Plating silver on the electrode design area on both sides of the ceramic electrothermal film to form electrodes;
[0029] Step 4: Weld...
Embodiment 1
[0039] In the preparation process of the nano-superlattice electrothermal film treatment solution, 1000g of antimony chloride, 10000g of tin chloride, 1500g of stannous chloride, 1500g of tin oxide, 1200g of stannous oxide, 800g of boron oxide and 1500g of bismuth oxide were weighed respectively , organic solvent 5000g; Ultrasonic 2h after described ethanol, acetic acid, methyl acetate mixes and makes mixed solution fully disperse uniformly to obtain organic solvent, wherein ethanol and acetic acid volume ratio are 4: 3, and ethanol and methyl acetate volume ratio are 9: 3; then add stannous oxide, tin oxide, tin chloride and the configured organic solvent into distilled water, stir vigorously for 10 hours, filter and separate to obtain solid and filtrate; add antimony chloride and stannous chloride into the organic solvent, Add an appropriate amount of hydrochloric acid dropwise, and stir vigorously for 1 hour to obtain solution A; add boron oxide and bismuth oxide to methyl a...
Embodiment 2
[0041] This example is basically the same as Example 1, except that during the preparation of the nano-superlattice electrothermal film treatment solution, 1200g of antimony chloride, 30000g of tin chloride, 1600g of stannous chloride, and 1700g of tin oxide were weighed respectively. , stannous oxide 1600g, boron oxide 900g, bismuth oxide 1800g, organic solvent 7000g; Described ethanol, acetic acid, methyl acetate are mixed and ultrasonic 3h makes mixed solution fully disperse evenly and obtain organic solvent, wherein ethanol and acetic acid volume ratio are 5 : 2, the volume ratio of ethanol to methyl acetate is 5: 2; then stannous oxide, tin oxide, tin chloride and the configured organic solvent are added to distilled water, vigorously stirred for 12h, filtered and separated to obtain solid and filtrate; Antimony chloride and stannous chloride were added to the organic solvent, and an appropriate amount of hydrochloric acid was added dropwise, and vigorously stirred for 2 h...
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