Environment-friendly plastic toy product preparation method
A technology for environmentally friendly plastics and toys, applied in the field of environmentally friendly materials, can solve the problems of aging resistance, plastic toys are not environmentally friendly, etc., and achieve the effects of improved high temperature resistance and aging resistance, good mechanical strength, and high hardness
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Embodiment 1
[0044] A method for preparing an environmentally friendly plastic toy product, comprising the following steps:
[0045] Step 1, prepare polyurethane prepolymer:
[0046] Weigh polycarbonate diol and diphenylmethane diisocyanate mixed prepolymerization reaction to prepare polyurethane prepolymer; wherein, the number average molecular weight of polycarbonate diol is 1000-4000; the reaction temperature of prepolymerization 50°C, the reaction time is 2h;
[0047] Step 2, prepare polyurethane elastomer:
[0048] Weigh 3,3-dichloro-4,4-diphenylmethanediamine and ethylene glycol according to the amount, first mix 3,3-dichloro-4,4-diphenylmethanediamine with polyurethane prepolymer Mixing, stirring and reacting at 78°C for 0.5-1h, then adding ethylene glycol, and then adding a catalyst for polymerization to prepare a polyurethane elastomer; wherein, the reaction temperature of the polymerization reaction is 78°C, and the reaction time is 4h; The mass ratio of 3,3-dichloro-4,4-diphe...
Embodiment 2
[0062] A method for preparing an environmentally friendly plastic toy product, comprising the following steps:
[0063] Step 1, prepare polyurethane prepolymer:
[0064] Weigh polycarbonate diol and diphenylmethane diisocyanate mixed prepolymerization reaction to prepare polyurethane prepolymer; wherein, the number average molecular weight of polycarbonate diol is 1000-4000; the reaction temperature of prepolymerization 45°C, the reaction time is 1h;
[0065] Step 2, prepare polyurethane elastomer:
[0066] Weigh 4,4-diphenylmethanediamine and 1,4-butanediol according to the amount, firstly mix 4,4-diphenylmethanediamine and polyurethane prepolymer, under the condition of 70~85℃ After stirring and reacting for 0.5-1 hour, add 1,4-butanediol, and then add a catalyst for polymerization reaction to prepare polyurethane elastomer; wherein, the reaction temperature of the polymerization reaction is 70-85°C, and the reaction time is 3-5 hours; The mass ratio of 4,4-diphenylmethan...
Embodiment 3
[0080] A method for preparing an environmentally friendly plastic toy product, comprising the following steps:
[0081] Step 1, prepare polyurethane prepolymer:
[0082] Weigh polycarbonate diol and isophorone diisocyanate mixed prepolymerization reaction to prepare polyurethane prepolymer; wherein, the number average molecular weight of polycarbonate diol is 1000-4000; the reaction temperature of prepolymerization The temperature is 60°C, and the reaction time is 3h;
[0083] Step 2, prepare polyurethane elastomer:
[0084] Weigh 3,5-dimethylthiotoluenediamine and 1,2-propanediol according to the amount, first mix 3,5-dimethylthiotoluenediamine and polyurethane prepolymer, under the condition of 70~85℃ After stirring and reacting for 0.5 to 1 hour, add 1,2-propanediol, and then add a catalyst for polymerization to prepare a polyurethane elastomer; wherein, the reaction temperature of the polymerization reaction is 70°C, and the reaction time is 3 hours; 3,5-dimethyl The ma...
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