Suspension auxiliary agent applied to grinding of large-size silicon wafer, and preparation method and application thereof

A suspension aid and large-scale technology, applied in the field of grinding suspension aids, can solve the problems of low grinding rate, increase the suspension performance of composite abrasives, scratches on the surface of silicon wafers, etc., to improve precision, improve grinding efficiency and production efficiency , the effect of reducing the loss layer

Active Publication Date: 2021-11-09
ZHEJIANG AUFIRST MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The object of the present invention is to propose a kind of suspending aid applied to the grinding of large-size silicon wafers for the low grinding rate of the current silicon wafer grinding liquid, which can easily produce surface scratches when used for silicon wafer grinding. Effectively increase the suspension performance of composite abrasives, and at the same time have good dispersion for different abrasives, avoiding the formation of abrasive agglomeration and abrasive hard precipitation in cyclic grinding

Method used

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  • Suspension auxiliary agent applied to grinding of large-size silicon wafer, and preparation method and application thereof
  • Suspension auxiliary agent applied to grinding of large-size silicon wafer, and preparation method and application thereof
  • Suspension auxiliary agent applied to grinding of large-size silicon wafer, and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] The suspension aid applied to the grinding of large-size silicon wafers of the present embodiment is composed of the following components (weight ratio):

[0050] Carboxyl modified bentonite: 1 part;

[0051] Polyether polyol: 5 parts;

[0052] Cocamidopropyl betaine: 0.1 parts;

[0053] Ammonium polyacrylate: 5 parts;

[0054] Isohexanediol: 15 parts;

[0055] Sebacic acid: 0.3 parts;

[0056] Deionized water: 73.6 parts;

[0057] The preparation method of the carboxyl-modified bentonite: first, take 100g of polyacrylic acid dispersant and add it into 1kg of deionized water, stir for 10 minutes until the mixture is uniform; heat the above solution to 60°C, and gradually add 200g of sodium-based bentonite at a speed of 100r / min , add within 10 minutes, then turn on high-speed homogeneous stirring at 4000r / min, and homogeneously stir for 60 minutes to prepare a carboxyl-modified bentonite gel; take 200g of the above-mentioned modified bentonite gel and add it to 1kg...

Embodiment 2-10、 comparative example 1-3

[0063] The composition and weight ratio of Examples 2-10 and Comparative Examples 1-3 are shown in Table 1, and the preparation method thereof is the same as that of Example 1.

[0064] Table 1, the components and weight ratios of the suspension aids used in the grinding of large-sized silicon wafers in Examples 2-10 and Comparative Examples 1-3.

[0065]

[0066]

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Abstract

The invention provides a suspension auxiliary agent applied to grinding of a large-size silicon wafer, a preparation method and application thereof. The suspension auxiliary agent comprises the following components in parts by weight: 0.5 to 5 parts of a hydrogen bond thixotropic agent, 0.5 to 5 parts of a suspension synergist, 0.1 to 1 part of a charge neutralizer, 0.5 to 10 parts of a dispersant, 10 to 20 parts of a lubricant, 0.1 to 0.5 part of an antirust agent, and 50 to 85 parts of water. The invention also discloses a preparation method of the suspension auxiliary agent. The preparation method comprises the following steps: sequentially adding the dispersant, the lubricant, the charge neutralizer and the antirust agent into the deionized water; heating to 40 DEG C, adding the hydrogen bond thixotropic agent into the solution, and standing to swell and stabilize the emulsion; and adding the suspension synergist into the solution to prepare the suspension auxiliary agent applied to large-size silicon wafer grinding. The prepared suspension auxiliary agent can effectively improve the suspension performance of the composite abrasive material, has good dispersity on different abrasive materials, and avoids abrasive material agglomeration and abrasive material hard precipitation in circulating grinding.

Description

technical field [0001] The invention relates to a grinding suspension aid technology, in particular to a suspension aid used in large-size silicon wafer grinding, its preparation method and application. Background technique [0002] With the development of semiconductor material technology, higher requirements are placed on the specifications and quality of silicon wafers, and the proportion of demand for large-diameter silicon wafers suitable for micro-processing will increase day by day. In the manufacturing process of large-size single crystal silicon wafers for semiconductors, the grinding technical indicators of silicon wafers are more stringent. It is necessary to make the silicon wafers have lower roughness, smaller thickness difference and lower depth of damage layer. The grinding process is The key step to maintain the quality of silicon wafers, and the suspension aid used in this step is one of the core technologies that affect the grinding index, which poses new t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K3/14
CPCC09K3/1463
Inventor 侯军李传强
Owner ZHEJIANG AUFIRST MATERIAL TECH CO LTD
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