Post-treatment method for Ni3Al-based single crystal alloy after welding
A single crystal-based, post-processing technology, applied in heat treatment furnaces, heat treatment equipment, welding equipment, etc., can solve problems such as difficult control of external stress conditions, uneven joint structure, large residual stress, etc., and achieve significant industrial application value and economy Benefits, simple post-processing method, and uniform joint structure
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[0031] In the present invention, the post-weld Ni 3 The preparation method of Al-based single crystal alloy preferably includes: Ni 3 Al-based single crystal alloys were brazed to obtain post-welded Ni 3 Al-based single crystal alloy; the brazing method is vacuum brazing.
[0032] In the present invention, Ni 3 Al-based single crystal alloys were brazed to obtain post-welded Ni 3 Al-based single crystal alloy.
[0033] In the present invention, the Ni 3 The type of the Al-based single crystal alloy is not particularly limited, and any type known to those skilled in the art may be used. In a specific embodiment of the present invention, the Ni 3 The Al-based single crystal alloy is specifically an IC21 alloy.
[0034] In the present invention, the Ni 3 The Al-based single crystal alloy is preferably heat-treated Ni 3 Al-based single crystal alloy; the present invention does not have any special limitation on the heat treatment process, it can be carried out by using th...
Embodiment 1
[0057] Cut the heat-treated IC21 single crystal rod into alloy blocks, grind the cross section and clean it ultrasonically for 15 minutes with acetone. Carry out butt joint tooling and fixation of two alloy blocks again, control gap to be 50 μ m, adopt platinum sheet to carry out spot welding and fix, then solder (B: 1wt%, Si: 3wt%, Ti: 7wt%, Al: 3wt%, Co : 9wt%, W: 4wt%, Cr: 11wt%, Ni: balance) coating and welding joint around, to obtain the IC21 alloy after pretreatment;
[0058] The IC21 after the pretreatment is placed in a vacuum heat treatment furnace and vacuumed to ≤7×10 -3 After Pa, raise the temperature from room temperature to 465°C at a heating rate of 10°C / min, and keep it for 30 minutes; ℃ to 1240℃, keep it warm for 120min, and then cool down with the furnace to obtain Ni after welding. 3 Al-based single crystal alloy;
[0059] The welded Ni 3 The Al-based single crystal alloy is placed in a tube furnace, heat-treated at 1050 °C for 10 h, and air-cooled to ob...
Embodiment 2
[0064] Cut the heat-treated IC21 single crystal rod into alloy blocks, grind the cross section and clean it ultrasonically for 15 minutes with acetone. Carry out butt joint tooling and fixation of two alloy blocks again, control gap to be 50 μ m, adopt platinum sheet to carry out spot welding and fix, then solder (B: 1wt%, Si: 3wt%, Ti: 7wt%, Al: 3wt%, Co : 9wt%, W: 4wt%, Cr: 11wt%, Ni: balance) coating and welding joint around, to obtain the IC21 alloy after pretreatment;
[0065] The IC21 after the pretreatment is placed in a vacuum heat treatment furnace and vacuumed to ≤7×10 -3 After Pa, raise the temperature from room temperature to 465°C at a heating rate of 10°C / min, and keep it for 30 minutes; ℃ to 1240℃, keep it warm for 120min, and then cool down with the furnace to obtain Ni after welding. 3 Al-based single crystal alloy;
[0066] The welded Ni 3 The Al-based single crystal alloy is placed in a tube furnace, heat-treated at a temperature of 1100 °C for 10 h, and...
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