Nanocrystalline flexible sheet and preparation method and application thereof
A nano-chip and crystal-flexible technology, applied in the field of nano-crystalline flexible sheet and its preparation, can solve the problem that the charging efficiency of MnZn ferrite and NiZn ferrite is not ideal, cannot have high saturation magnetic induction at the same time, and cannot meet the requirements of use. To achieve the effect of promoting Fe enrichment and nucleation, improving the uniformity of the microstructure, and increasing the ability to form amorphous
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[0054] The present invention also provides a method of preparing a nanocrystalline flexible sheet, in some embodiments, the relaxation treatment has a temperature of from 280 to 380 ° C, which may be any value of this, such as 300 ° C, 320 ° C, 350 ° C. , 360 ° C, etc., the present invention is not limited, further, when the relative treatment temperature is preferably 300-350 ° C, the obtained nanocrystalline flexible sheet is better, the relaxation treatment is 300-350 ° C. Any value between, for example, 310 ° C, 325 ° C, 335 ° C, 345 ° C, etc., the present invention is not limited thereto.
[0055] In some embodiments, the relaxation treatment is carried out at a magnetic field strength of 10-800 mT, and when the magnetic field strength is 500-800mt, the obtained nanocrystalline flexible sheet is better, and the magnetic field strength is between 500.00mm. Any value, such as 550 mt, 600 mt, 650 mt, 700mt, 750mt, etc., the present invention is not limited.
[0056] The technica...
Example Embodiment
[0057] Example 1
[0058] This embodiment provides a nanocrystalline flexible sheet comprising Fe, Cu, Si, B, Nb, Mo, Cu, Si, B, Nb, Mo and Y, atomic percentage of 76.1 at%, 0.9 at%, 13.5 at%, 7.5at, respectively. %, 1.2AT%, 0.6At% and 0.2 at%, ie molecular formula Fe 76.1 Cu 0.9 Si 13.5 B 7.5 NB 1.2 Mo 0.6 Y 0.2 .
[0059] The preparation method of the above nanocrystalline flexible sheet includes the steps of:
[0060] (1) Raw materials, copper raw materials, silicon feedstock, boron iron alloy ingot raw materials, molybdenum iron alloy ingot raw materials, and yttrium materials, in accordance with the percentage of the above-mentioned percentage, cooling at 1320 ° C for 45min, cooled, to obtain alloy ingots; then heating alloy ingots After the molten liquid state, the neutral nozzle is sprayed to the rotating copper bar to obtain a nano-crystal precursor (the process is fast quenching quenching); wherein the width of the nanocrystalline precursor is 60 mm, with a belt thickness...
Example Embodiment
[0063] Example 2
[0064] This embodiment provides a nanocrystalline flexible sheet comprising Fe, Cu, Si, B, NB, Mo, and HO, atomic percentage of 76.4 at%, 0.6 at%, 13At%, 8 at%, respectively, 1.2AT%, 0.5 at% and 0.1 at%, ie the molecular formula Fe 76.4 Cu 0.6 Si 13 B 8 NB 1.2 Mo 0.5 HO 0.1 .
[0065] The preparation method of the above nanocrystalline flexible sheet is in Example 1.
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