Manufacturing method of anti-static filtering material and anti-static filtering material
A technology of filter material and production method, which is applied in the field of materials to achieve the effect of avoiding electrostatic hazards
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Embodiment 1
[0035] 1. Modified nano tourmaline
[0036] The nano-tourmaline that takes 5g joins and joins in the 30ml toluene and the water mixed solvent that solid-liquid ratio is 1:6, is placed on there-necked flask then, adds coupling agent (isopropyl trititanic acid) in flask, makes in whole The mass fraction of the coupling agent in the mixture system is 2%. Add the reaction solvent toluene to the flask, and continue the reaction in an oil bath at 90°C for 3 hours. Then wash with distilled water and absolute ethanol for 3 times, put it in a centrifuge at a speed of 8000r / min for centrifugation, and dry it at 80°C after centrifugation to obtain surface-modified tourmaline, and grind it to 10nm particle size;
[0037] 2. Preparation of PTFE / tourmaline blend fiber
[0038] PTFE micropowder and modified tourmaline are mixed according to a certain mass ratio, and then mixed with aviation kerosene, PTFE micropowder: modified tourmaline: aviation kerosene = 17:3:5.3, and the mixed powder...
Embodiment 2
[0044] 1. Modified nano tourmaline
[0045] The nano-tourmaline that takes 7g joins and joins in the 42ml toluene and the water mixed solvent that solid-liquid ratio is 1:6, is placed on there-necked flask then, adds coupling agent (isopropyl trititanic acid) in flask, makes in whole The mass fraction of the coupling agent in the mixture system is 1%. Add the reaction solvent toluene to the flask, and continue the reaction in an oil bath at 90°C for 3 hours. Then wash with distilled water and absolute ethanol for 3 times, put it in a centrifuge at a speed of 5000r / min for centrifugation, and dry it at 60°C after centrifugation to obtain surface-modified tourmaline, and grind it to 60nm particle size.
[0046] 2. Preparation of PTFE / tourmaline blended fiber
[0047] PTFE micropowder and modified tourmaline are mixed according to a certain mass ratio, and then mixed with aviation kerosene, PTFE micropowder: modified tourmaline: aviation kerosene = 17:3:5.3, and the mixed powd...
Embodiment 3
[0053] 1. Modified nano tourmaline
[0054] The nano-tourmaline that takes by weighing 10g joins in the 60ml toluene and the water mixed solvent that solid-liquid ratio is 1:6, is placed in there-necked flask then, adds coupling agent (isopropyl trititanic acid) in flask, makes in whole The mass fraction of the coupling agent in the mixture system is 3%. Add the reaction solvent toluene to the flask, and continue the reaction in an oil bath at 90°C for 3 hours. Then wash with distilled water and absolute ethanol for 3 times, put it in a centrifuge at a speed of 6000r / min for centrifugation, and dry it at 70°C after centrifugation to obtain surface-modified tourmaline, and grind it to 100nm .
[0055] 2. Preparation of PTFE / tourmaline blended fiber
[0056] PTFE micropowder and modified tourmaline are mixed according to a certain mass ratio, and then mixed with aviation kerosene, PTFE micropowder: modified tourmaline: aviation kerosene = 17:3:5.3, and the mixed powder is age...
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