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Preparation method and application of high-temperature alloy bar

A technology for high-temperature alloys and alloy bars, applied in the field of metallurgy, can solve problems such as insufficient strength and poor plasticity, and achieve the effect of improving high-temperature mechanical properties, good plasticity, and good oxidation resistance and corrosion resistance.

Active Publication Date: 2022-03-25
北冶功能材料(江苏)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] For this reason, the present invention provides a preparation method and application of superalloy rods to solve technical problems such as insufficient strength and poor plasticity faced by CrCoNi medium entropy alloys

Method used

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  • Preparation method and application of high-temperature alloy bar
  • Preparation method and application of high-temperature alloy bar
  • Preparation method and application of high-temperature alloy bar

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preparation example Construction

[0043] The preparation method of the high-temperature superalloy bar specifically includes the following steps:

[0044] Step 1. Raw materials of Cr, Co, Ni, Fe, Mo, W, and C are mixed according to the proportion, put into a vacuum induction furnace for melting, high-temperature refining for 25-35 minutes, and the refining temperature is 1600-1650°C, and cast into an alloy ingot .

[0045] Step 2. Forging the alloy ingot. The heating temperature for forging is 1100-1200°C. When forging an electrode rod, the forging ratio is 4-6. Forging an alloy electrode rod, and then remelting. The remelting uses a vacuum electric arc furnace for remelting Or vacuum electroslag remelting to crystallize into remelted steel ingots.

[0046] Step 3: Forging the remelted and remelted steel ingot, the forging heating temperature is 1100-1200°C, the forging ratio is 4-6 when forging an alloy billet, and hot rolling the alloy billet, the hot-rolling temperature range is 1150-1200°C 1250°C, the ho...

Embodiment 1-3

[0049] A method for preparing a superalloy rod according to this embodiment, the method specifically includes the following steps:

[0050] According to the composition ratio of alloys 1 to 3 shown in Table 1, the ingredients were mixed, and the C, Co, Ni, Cr, Mo, W, and Fe raw materials were weighed, put into a 50kg vacuum induction melting furnace for melting, and refined at high temperature for 25 minutes , the refining temperature is 1650°C, and cast into alloy ingots.

[0051] The alloy ingots were forged into alloy electrode rods at a temperature of 1100 °C with a forging ratio of 4. Then remelt in a vacuum electric arc furnace and crystallize into a remelted alloy ingot;

[0052] The remelted alloy ingot is forged, the forging temperature is 1100°C, the blank is forged into an alloy billet, and the forging ratio is 4. After surface grinding and defect detection, the alloy billet is hot rolled into an alloy billet at a temperature of 1150°C, the hot rolling reduction r...

Embodiment 4-6

[0061] A method for preparing a superalloy rod according to this embodiment, the method specifically includes the following steps:

[0062] According to the proportion of alloys 4 to 6 shown in Table 3, the ingredients were mixed respectively, and the raw materials of C, Co, Ni, Cr, Mo, W, and Fe were weighed, put into a 50kg vacuum induction melting furnace for melting, and refined at high temperature for 30 minutes. The refining temperature is 1620°C and cast into alloy ingots.

[0063] The alloy ingot was forged into an alloy electrode rod at a temperature of 1150 °C, and the forging ratio was 5. It is then remelted in a vacuum electric arc furnace and crystallized into a remelted alloy ingot.

[0064] The remelted alloy ingot is forged, the forging temperature is 1150°C, the blank is forged into an alloy billet, and the forging ratio is 5. After surface grinding and defect detection, the alloy billet is hot rolled into an alloy billet at a temperature of 1200, the hot ro...

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Abstract

The invention discloses a preparation method of a high-temperature alloy bar. The method comprises the following steps that raw materials including Cr, Co, Ni, Fe, Mo, W, C, Mo and W are taken according to a certain proportion to be mixed, smelted, refined and cast into an alloy ingot; forging the alloy ingot to form an alloy electrode bar, and remelting and crystallizing the alloy electrode bar to form a remelted steel ingot; carrying out forging and hot rolling on the remelted steel ingot to obtain an alloy bar blank, and carrying out bar cold drawing on the alloy bar blank to form a primary alloy bar; and aging treatment is conducted on the primary alloy bar, and the alloy bar is obtained. The prepared high-temperature alloy bar has reasonable composition proportion, wide hot working window and heat treatment system, and the prepared high-temperature alloy bar has high high-temperature strength, high elastic modulus and good oxidation resistance and corrosion resistance, and is a candidate material for aero-engines and industrial gas turbine hot end components.

Description

technical field [0001] The invention relates to the technical field of metallurgy, in particular to a preparation method and application of a superalloy rod. Background technique [0002] High-entropy alloy is a new type of alloy material developed in recent years that is different from traditional alloys. It is composed of 5 to 13 main elements, and the constituent elements have equal or approximately equal atomic ratios. After the solidification of multi-principal high-entropy alloys, complex intermetallic compounds will not be formed, but simple FCC or BCC solid solutions will be formed. High-entropy alloys have thermodynamic high-entropy effects, structural lattice distortion effects, kinetic hysteretic diffusion effects, and performance cocktail effects. Utilizing these effects and rationally designing the composition of the alloy, good comprehensive properties such as high hardness, high elasticity, high strength, good wear resistance, corrosion resistance and high te...

Claims

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Application Information

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IPC IPC(8): C22C1/02C22C30/00C22B9/18C22B9/20
CPCC22C1/02C22C30/00C22B9/18C22B9/20
Inventor 安宁赵文倩薛佳宁邓睿安杨钟文靖高杨张荣
Owner 北冶功能材料(江苏)有限公司