Supercharge Your Innovation With Domain-Expert AI Agents!

Method for detecting content of caprolactone in acrylic resin

A technology of acrylic resin and detection method, which is applied in the field of detection and analysis, can solve the problem that the detection of caprolactone content does not have any national standards and analysis methods, and affects the quality of acrylic resin products, so as to reduce costs, improve detection accuracy, and improve detection. efficiency effect

Pending Publication Date: 2022-04-01
山东惠分仪器有限公司
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The hardness, flexibility and cohesiveness of acrylic resin can be changed by caprolactone, but when the content of caprolactone exceeds 2000ug / ml, will directly affect the product quality of acrylic resin, therefore, need the content of caprolactone in acrylic resin However, at present, there are no national standards and analytical methods for the detection of caprolactone content in acrylic resins

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for detecting content of caprolactone in acrylic resin
  • Method for detecting content of caprolactone in acrylic resin
  • Method for detecting content of caprolactone in acrylic resin

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0029] see Figure 1~3 , in the embodiment of the present invention, the detection method of caprolactone content in acrylic resin, comprises the following steps:

[0030] S1. Sample preparation: the solvent selected by the gas chromatograph is chromatographic grade pure ethyl acetate, and the column material of the gas chromatograph is a quartz capillary column;

[0031] S2. Setting of chromatographic conditions: the column temperature of the gas chromatograph is set to 90°C (5min), 10°C / min, 280°C (10min), the temperature of the injector is 280°C, the temperature of the detector is 280°C, and the carrier gas is nitrogen The flow rate is 30mL / min, the air flow rate is 300 mL / min, the hydrogen flow rate is 30mL / min, and the injection volume is 0.5mL;

[0032] S3, detection operation: start the gas chromatograph, then mix the acrylic resin liquid sample and ethyl acetate evenly, and perform data analysis and processing, and then calculate the content of caprolactone in the acr...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to the technical field of detection and analysis, and discloses a method for detecting the content of caprolactone in acrylic resin, which comprises the following steps: S1, sample preparation; s2, setting chromatographic conditions; s3, detection operation: starting a gas chromatograph, then uniformly mixing the acrylic resin liquid sample with ethyl acetate, carrying out data analysis processing, and then calculating to obtain the content of caprolactone in the acrylic resin; s4, drawing a standard curve; s5, qualitative analysis of caprolactone; s6, quantitative result calculation of caprolactone: directly obtaining the concentration of caprolactone according to the caprolactone standard curve, and calculating the concentration of caprolactone in the acrylic resin; and S7, testing precision and accuracy. According to the present invention, the acrylic resin sample is dissolved by using the ethyl acetate, the gas chromatograph with the hydrogen flame ionization detector is adopted, the caprolactone content is calculated by using the external standard method after the peak area quantitative analysis, such that the detection efficiency and the detection precision can be improved, the cost can be reduced, the safety and the environmental protection are provided, and the harm to the human body is avoided.

Description

technical field [0001] The invention relates to the technical field of detection and analysis, in particular to a detection method for caprolactone content in acrylic resin. Background technique [0002] Acrylic resin is a commonly used paint component at present. It has many outstanding excellent properties, such as light color, excellent weather resistance, good decoration, comprehensive performance, outstanding three-proof performance, many varieties, wide range of uses, and easy to obtain raw materials. Reasonable price, etc., and widely used. [0003] The hardness, flexibility and cohesiveness of acrylic resin can be changed by caprolactone, but when the content of caprolactone exceeds 2000ug / ml, will directly affect the product quality of acrylic resin, therefore, need the content of caprolactone in acrylic resin Detect, yet, at present, the detection of caprolactone content in acrylic resin does not have any national standard and analytical method. Contents of the ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): G01N30/02G01N30/64
Inventor 杨文杨中元史德庆李峰耿文涛
Owner 山东惠分仪器有限公司
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2025 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com