Process for preparing porous supporter material from multiple emulsion template
A porous scaffold and multiple emulsion technology, applied in the field of preparation of biomedical materials, can solve the problems of inaccurate control of pore size and distribution, achieve good applicability, ensure mechanical strength, and improve affinity
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example 1
[0017] Example 1: Take 3g of polyhydroxybutyrate and put it into 90ml of chloroform, stir until fully dissolved, transfer the solution to a 100ml volumetric flask after filtration, add chloroform to the mark, and obtain 100ml of polyhydroxybutyrate chloroform solution A; Dissolve 1.7g of Sorbitan trioleate Span85 in 60ml of deionized water at 70°C to obtain a stable template emulsion B; take 20ml of solution A and 0.5ml of solution B and mix together, stir until the solution is evenly mixed and stable, then let it stand for defoaming , scratch the film on the glass plate. The obtained membrane is naturally dried at room temperature, then soaked in solvent cyclohexane to remove the template, washed repeatedly with water, and dried to constant weight in a vacuum drying oven to prepare a porous monolithic membrane. Pour 2~3ml of chloroform on the tetrafluoroethylene plate to make it fully spread, lightly place the two overlapping monolithic membranes on the tetrafluoroethylene pl...
example 2
[0019] Take 1g of polyhydroxybutyrate and put it into 90ml of chloroform, stir until fully dissolved, transfer the solution to a 100ml volumetric flask after filtration, add chloroform to the mark, and obtain 100ml of polyhydroxybutyrate chloroform solution A; take sorbitan tris Dissolve 0.7g of Span85 oleate in 60ml of deionized water at 70°C to obtain a stable template emulsion B; take 20ml of solution A and 0.5ml of B and mix together, stir until the solution is evenly mixed and stable, then let it stand for defoaming, and put it on a glass plate Scratch film on. The obtained membrane is naturally dried at room temperature, then soaked in solvent cyclohexane to remove the template, washed repeatedly with water, and dried to constant weight in a vacuum drying oven to prepare a porous monolithic membrane. Pour 2~3ml of chloroform on the tetrafluoroethylene plate to make it fully spread, lightly place the two overlapping monolithic membranes on the tetrafluoroethylene plate, p...
example 3
[0021] Take 5g of polyhydroxybutyrate and put it into 90ml of chloroform, stir until fully dissolved, transfer the solution to a 100ml volumetric flask after filtration, add chloroform to the mark, and obtain 100ml of polyhydroxybutyrate chloroform solution A; take sorbitan tris Dissolve 0.1g of Span85 oleate in 60ml of deionized water at 70°C to obtain a stable template emulsion B; take 20ml of solution A and 0.5ml of B and mix together, stir until the solution is evenly mixed and stable, then let it stand for defoaming, and put it on a glass plate Scratch film on. The obtained membrane is naturally dried at room temperature, then soaked in solvent cyclohexane to remove the template, washed repeatedly with water, and dried to constant weight in a vacuum drying oven to prepare a porous monolithic membrane. Pour 2~3ml of chloroform on the tetrafluoroethylene plate to make it fully spread, lightly place the two overlapping monolithic membranes on the tetrafluoroethylene plate, p...
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