Cross-linked low medium electrical property high polymer material and film, base plate and electronic part using the same
A polymer material, low dielectric technology, applied in the direction of circuit substrate materials, printed circuit components, electrical components, etc., can solve the problem of high dielectric constant, unsatisfactory properties, and polyimide resin not practical Level and other issues, to achieve the effect of improving mechanical properties, dielectric constant and dielectric loss tangent, and good adhesion
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Synthetic example 1
[0053] Add 85 parts by weight of dicyclohexyl fumarate (di-CHF) and 15 parts by weight of glycidyl acrylate (GAA) to a glass ampoule, then add 1 part by weight of azobisisobutyronitrile (AIBN) as free radical polymerization initiator, and then add 10 parts by weight of refined benzene into the glass ampoule, fully carry out nitrogen replacement, repeatedly perform decompression and degassing, and seal the ampoule under vacuum. Then, this ampoule was placed in a thermostat at 40° C., and kept for 72 hours. After the polymerization is completed, the content liquid is added to a large amount of methanol, the polymer is precipitated and separated, and dried under reduced pressure to obtain the target copolymer.
Synthetic example 2
[0055] Except that glycidyl methacrylate (GMA) was used instead of GAA in Synthesis Example 1, the other was the same to prepare a copolymer.
Synthetic example 3
[0057] A copolymer was obtained in the same manner as in Synthesis Example 1 except that 3,4-epoxycyclohexylmethanol acrylate (ECHMA) (manufactured by Daicel Chemical Industry Co., Ltd., trade name: CYCLOMER A 200) was used instead of GAA.
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Abstract
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