Prepn of polyvinylidene difluoride film for secondary lithium ion battery
A polyvinylidene fluoride, secondary battery technology, used in battery pack parts, circuits, electrical components, etc.
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Embodiment 1
[0015] First, tetrahydrofuran (THF) and acetone are mixed according to a weight ratio of 1:1 to form a composite component solvent, then water and ethanol are mixed according to a weight ratio of 1:1 to form a composite component non-solvent, and the solvent and non-solvent are mixed according to 84: After mixing evenly at a weight ratio of 8, mix according to the weight ratio of polyvinylidene fluoride-hexafluoropropylene (PVDF-HFP): mixture of mixed component solvent and mixed component non-solvent = 8:92, at 40°C-70°C Stir at constant temperature for 2-6 hours to obtain a clear and viscous sol, which can be scraped on a smooth glass plate or coated with aluminum foil on a coating machine, let the solvent and non-solvent evaporate naturally, and remove the dried film The polyvinylidene fluoride film of the present invention can be obtained by placing it in an environment of 60°C and drying for 24 hours.
Embodiment 2
[0017] First, tetrahydrofuran (THF) and acetone are mixed according to the weight ratio of 1:1 to form a composite component solvent, and after the composite component solvent and water are mixed uniformly according to a weight ratio of 84:8, according to polyvinylidene fluoride-hexafluoropropylene ( PVDF-HFP): mixed component solvent and water mixture = 8:92 weight ratio mixed, stirred at a constant temperature of 40°C-70°C for 2-6 hours to obtain a clear and viscous sol, scraped on a smooth glass plate Coating or coating on a coating machine with aluminum foil as a carrier, let the solvent and non-solvent volatilize naturally, remove the dried film and put it in an environment of 60 ° C for 24 hours to obtain the polyvinylidene fluoride film of the present invention . .
Embodiment 3
[0019] First, water and ethanol are mixed according to a weight ratio of 1:1 to form a composite component non-solvent, and after acetone and a composite component non-solvent are mixed uniformly according to a weight ratio of 84:8, the polyvinylidene fluoride-hexafluoropropylene (PVDF -HFP): acetone and mixed component non-solvent mixture = 8: 92 weight ratio mixing, constant temperature stirring at 40°C-70°C for 2-6 hours, to obtain a clear viscous sol, scrape on a smooth glass plate Coating or coating on a coating machine with aluminum foil as a carrier, let the solvent and non-solvent volatilize naturally, remove the dried film and put it in an environment of 60 ° C for 24 hours to obtain the polyvinylidene fluoride film of the present invention . .
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