Water suspension acetamiprid nano capsule prepn and its preparing method
A technology of nanocapsules and water suspension, which is applied in the field of acetamiprid water suspension nanocapsules and pesticide formulations, which can solve the problems of pesticide residues, waste of resources, decomposition and waste, etc., to reduce acute toxicity, improve utilization rate, and stabilize sex-enhancing effect
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Embodiment 1
[0065]Dissolve 0.1g of ammonium persulfate in 20g of water (divided into two parts by 4:1), stand-by; 0.5g of acetamiprid is dissolved in the mixed monomer of 7g of styrene, 8g of butyl acrylate, and 0.2g of acrylic acid; Dissolve 6g of OP-40 and 1g of sodium lauryl sulfate in 50g of 2% polyvinyl alcohol aqueous solution, put it into a container with stirring, add the mixed monomers dissolved in acetamiprid under stirring, and disperse into an emulsion , into the reaction vessel. Heat to keep the temperature at 70±2°C, add the first part of initiator, react for 6 hours, keep warm for 1 hour, and prepare the seed emulsion; add 1.5g of styrene, 1.5g of butyl acrylate, 2g of toluene diisocyanate mixed monomer and Add the second initiator dropwise for 1 hour, keep warm for 2 hours, cool down; add additives, and discharge. The content of acetamiprid in the product was 0.5%.
Embodiment 2
[0067] Dissolve 0.1g of potassium persulfate in 10g of water (divided into two parts according to 4:1), dissolve 1g of acrylamide in 10g of water, and set aside; dissolve 1g of acetamiprid in a mixed monomer of 4g of ethyl acrylate and 7g of butyl acrylate In; 5g OP-40, 4g sodium lauryl sulfate, 4g sodium polymethacrylate are dissolved in 60g water, put into a container with stirring, under stirring, add the mixed monomer that dissolves acetamiprid, Disperse into an emulsion and put it into a reaction vessel. Heat and keep the temperature at 70±2°C, add the first initiator and acrylamide aqueous solution, react for 6 hours, keep warm for 1 hour, and prepare the seed emulsion; add 1g ethyl acrylate, 1g butyl acrylate, 2g 4,4' - diphenylmethane diisocyanate mixed monomer, dropwise for 1 hour, keep warm for 2 hours, cool down; add additives, discharge. The content of acetamiprid in the product was 0.9%.
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