Process for preparing proton exchange film fuel cell multi component catalyst
A proton exchange membrane, fuel cell technology, applied in catalyst carriers, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problems of limiting the practical speed of fuel cells, high cost, lack of resources, etc., to improve the anti-CO Poisoning ability, less agglomeration, high purity effect
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example 1
[0021] 1) 20 parts of activated carbon, 30 parts of chloroplatinic acid, 30 parts of ruthenium trichloride, and 20 parts of cerium oxide are added to a closed container loaded with 75% deionized water to form a premix;
[0022] 2) The premix was reacted in a nitrogen atmosphere at 200°C and a pressure of 2.5Mpa for 6 hours, and then cooled to room temperature;
[0023] 3) Add 2 parts of sodium thiosulfate and treat at 140° C. for 4 hours to evenly fix platinum, ruthenium and cerium on the original position of the reduction reaction;
[0024] 4) Filtrating, washing and drying the slurry formed above to obtain a PtRuCe / C multi-component catalyst.
example 2
[0026] 1) 25 parts of carbon nanotubes, 50 parts of platinum chloride, 10 parts of ruthenium oxide, and 15 parts of samarium oxide are added to a closed container in which 80% deionized water has been added to form a premix;
[0027] 2) The premix was reacted in an argon atmosphere at 150°C and a pressure of 2Mpa for 8 hours, and then cooled to room temperature;
[0028] 3) adding 4 parts of sodium dithionite, treating at 120°C for 6 hours, evenly fixing platinum, ruthenium and samarium on the original position of the reduction reaction;
[0029] 4) Filtrating, washing and drying the slurry formed above to obtain a PtRuSm / C multi-component catalyst.
example 3
[0031] 1) Add 20 parts of activated carbon, 25 parts of platinum oxide, 25 parts of ruthenium oxide, and 30 parts of yttrium oxide into a closed container that has been dewatered by 80% to form a premix;
[0032] 2) The premix was reacted in a nitrogen atmosphere at 300°C and a pressure of 2Mpa for 6 hours, and then cooled to room temperature;
[0033] 3) adding 2 parts of sodium formate, and treating at 200° C. for 2 hours, evenly fixing platinum, ruthenium and yttrium on the original position of the reduction reaction;
[0034] 4) Filter, wash and dry the slurry formed above to obtain a PtRuY / C multi-component catalyst.
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