Transparent composite composition
A composite material and composition technology, applied in thin material handling, instrumentation, transportation and packaging, etc., can solve problems such as unsatisfactory heat resistance and solvent resistance
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Embodiment 1
[0075] E-glass glass cloth (thickness 50 μm, refractive index 1.560, manufactured by Unitika cloth, E06B (#1080) is burned to remove organic matter, and then treated with acryloxypropyltriethoxysilane (alkylsilane) The resin composition (refractive index 1.560 after the cross-linking) that is made of following compound is impregnated on this glass cloth and degasses. Said compound is bicyclic dienyl diacrylate (formula 1) (Toagosei Co., Ltd. ), M-203, cross-linked refractive index 1.527) 58 parts by weight, bis[4-(acryloyloxyethoxy)phenyl] sulfide (Formula 3) (Toagosei Co., Ltd. trial product, TO-2066, crosslinked refractive index 1.606) 42 parts by weight, and photopolymerization initiator (1-hydroxy-cyclohexyl-phenyl-ketone (manufactured by Ciba Specialty Chemicals, Irgacure 184) 0.5 parts by weight. The obtained glass cloth Laminated with resin / glass cloth / resin / glass cloth / resin, sandwiched between glass plates that have been released from the mold, and irradiated at about...
Embodiment 2
[0077] Prepare 53 parts by weight of norbornane dimethylol diacrylate (formula 2) (Toya Gosei Co., Ltd. trial product, refractive index after crosslinking: 1.520), bis[4-(acryloyloxyethoxy)benzene base] sulfide (Formula 3) (Toagosei Co., Ltd. trial product, TO-2066, after crosslinking, the refractive index is 1.606) 47 parts by weight, and a resin composition composed of 0.5 parts by weight of photopolymerization initiator (refractive index after crosslinking Rate 1.560) as a resin composition, it was impregnated on the same glass cloth as in Example 1 and defoamed. This glass cloth was laminated in the same manner as in Example 1, and then irradiated with ultraviolet light and heat-treated to obtain a sheet-shaped plastic substrate (thickness: 0.2 mm). The glass filler content of the substrate was 30% by weight.
Embodiment 3
[0079] Burn E-glass glass cloth (thickness 100 μm, refractive index 1.560, manufactured by Unitika cloth, E10A (#2117) to remove organic matter, and then treat it with acryloxypropyltriethoxysilane (alkylsilane) On this glass cloth, impregnate the resin composition of the same composition as embodiment 1 and carry out defoaming.This glass cloth is clamped on the glass plate through release process, irradiates about 500mJ / cm from both sides 2 UV light cures it. After heating in a vacuum oven at about 100° C. for 3 hours, and then heating at about 250° C. for 3 hours, a thin plastic substrate with a thickness of 0.1 mm was obtained. The glass filler content of the substrate was 50% by weight.
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Abstract
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