Epoxy molding compound and preparation method thereof
An epoxy molding compound and epoxy technology, applied in the field of integrated circuit packaging, can solve the problems of unsatisfactory thermal properties, mechanical properties and electrical properties of epoxy molding compounds
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[0037] Example 1
[0038] The purpose of this example is to study the influence of the amount of fused silicon micropowder on the thermal, mechanical, electrical and other properties of EMC. That is, 5% (mass percentage) of coupling agent solution was used to couple and modify the molten silicon micropowder that was ball-milled for 24h (2μm) (the silicon micropowder with an average particle size of 2μm obtained after ball-milling for 24h). The linear expansion coefficient, thermal conductivity, flexural strength, elastic modulus, dielectric constant and dielectric loss of EMC of the amount of silicon micro-powder.
[0039]
[0040] Electronic analytical balance; JJ-3 constant temperature electric stirrer; DK-8B type electric heating constant temperature water tank; KQ5200DE type numerical control ultrasonic cleaner; NP-C-20-1500 in-line ultrasonic disperser; DZF-6020 vacuum drying oven.
[0041] Experimental steps:
[0042] 1. Weigh a certain amount of silicon micropowder...
Example Embodiment
[0057] Example 2
[0058] The purpose of this example is to study the effect of the particle size of the fused silica micropowder on the thermal and mechanical properties of EMC. That is, 5% coupling agent solution was used to couple and modify the molten silicon micropowder ball milled for 16h, 24h, 30h, 38h, 48h, and the linear expansion coefficient, flexural strength, elastic modulus of EMC with an addition amount of 50% were tested. quantity.
[0059] Experimental materials and procedures:
[0060] Except that the addition amount of molten silicon micropowder is fixed at 50%, the rest is the same as that in Example 1.
[0061] Experimental results and discussion:
[0062] Table 2 Influence of particle size of fused silica micropowder on thermal and mechanical properties of EMC
[0063] Silica powder particle size (μm)
[0064] no filler
[0065] In terms of thermal properties, it can be seen from Table 2 that under the same addition amount of 50%, t...
Example Embodiment
[0068] Example 3
[0069] The purpose of this example is to study the influence of different types of silicon micropowder on the EMC linear expansion coefficient. That is, 5% coupling agent solution is used to couple and modify kaolin tailings silicon micropowder, high-purity crystalline silicon powder, molten silicon micropowder, and silicon micropowder after secondary firing, and the test dosage is 60%. When the EMC coefficient of linear expansion and thermal conductivity.
[0070] Experimental materials and procedures
[0071] Except that the addition amount of various types of silicon micropowder is fixed at 60%, the others are the same as in Example 1.
[0072] Experimental Results and Discussion
[0073] Table 3 Effects of different silicon micropowders on EMC linear expansion coefficient and thermal conductivity
[0074] Types of microsilica
[0075] Silicon powder after secondary firing (10μm)
[0076] It can be seen from Table 3 that the effect...
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