Method for preparing Pt-Ru-NI/C catalyst in use for fuel cell of direct alcohols
A fuel cell and catalyst technology, applied in catalyst activation/preparation, physical/chemical process catalysts, chemical instruments and methods, etc., can solve the problems of expensive battery catalysts and limited resources
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specific Embodiment approach 1
[0005] Specific Embodiment 1: This embodiment is achieved through the following steps: 1. Add the carbon carrier that has undergone hydrophilic treatment into the mixed solution of deionized water and isopropanol, disperse evenly, and make a carbon-containing slurry; 2. Put the Pt , Ru and Ni compound precursors are added to the uniformly dispersed carbon-containing slurry, so that the Pt, Ru and Ni compound precursors are evenly dispersed on the carbon carrier; 3. The uniformly dispersed carbon-supported Pt, Ru and Ni compound precursor slurry Adjust the pH value to 3-10; 4. Heat the obtained slurry to 50-90°C, add a reducing agent, and reduce for 1-5 hours to form a reducing solution; 5. Rinse the reducing solution with ultra-pure water, It can be dried under vacuum condition at ℃ for 1-6 hours (that is, the Pt-Ru-Ni / C three-way catalyst is prepared). The metal molar ratio of Pt, Ru and Ni is 4-7:2-5:1-3. The reducing agent is sodium borohydride or potassium borohydride. T...
specific Embodiment approach 2
[0006] Embodiment 2: In step 3 described in this embodiment, the pH value is adjusted to 6-8. Other steps are the same as in the first embodiment.
specific Embodiment approach 3
[0007] Embodiment 3: The temperature of the slurry in step 4 described in this embodiment is 60-90°C. Other steps are the same as in the first embodiment.
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