Method for detecting the quality of the medicine combination for treating cerebral apoplexy and vasculitis
A quality detection method and composition technology, which is applied in the direction of drug combinations, pharmaceutical formulas, measuring devices, etc., can solve the problems of undisclosed quality detection methods, poor stability of ferulic acid, undisclosed drug ratio relationship and preparation methods, etc.
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[0213] Example 1:
[0214] Astragalus 420kg, Angelica 530kg, Codonopsis 420kg, Scrophulariaceae 530kg, Honeysuckle 420kg, Dendrobium 530kg, Achyranthes 420kg, Licorice 530kg;
[0215]Add the raw material medicine into the multifunctional extraction tank, add 6 times the amount of water, heat and cook for 0.5 hours, and start timing when the temperature in the pot reaches 100°C; after filtering, the filtrate I is obtained and input into the liquid storage tank for standby; the medicine residue is added again 4 times the amount of water is decocted for 0.5 hours, filtered, and combined with filtrate I to obtain filtrate II, which is discarded; the filtrate II is input into the double-effect concentrator, the temperature is controlled below 70℃, and the vacuum degree is above -0.05Mpa Heat and concentrate to 50~60℃, relative density 1.10~1.29, collect thick paste I; take thick paste I and put it in an alcohol precipitation tank, add ethanol to 70% alcohol content, stir well, let stan...
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[0219] Example 2:
[0220] Astragalus 480kg, Angelica 480kg, Codonopsis 480kg, Scrophulariaceae 480kg, Honeysuckle 480kg, Dendrobium 480kg, Achyranthes 480kg, Licorice 480kg;
[0221] Add the raw material medicine to the multifunctional extraction tank, add 5 times the amount of water, heat and cook for 1.5 hours, and start timing when the temperature in the pot reaches 100°C; after filtering, the filtrate I is obtained and input into the storage tank for standby; the medicine residue is added again 3 times the amount of water is decocted for 1 hour, filtered, and combined with filtrate I to obtain filtrate II, which is discarded; the filtrate II is input into the double-effect concentrator, the temperature is controlled below 70℃, and the vacuum degree is above -0.05Mpa Heat and concentrate to 50~60℃, relative density 1.10~1.29, collect thick paste I; take thick paste I and put it in an alcohol precipitation tank, add ethanol to 60% alcohol content, stir well, let stand for more ...
Example Embodiment
[0225] Example 3:
[0226] Astragalus 480kg, Angelica 480kg, Codonopsis 480kg, Scrophulariaceae 480kg, Honeysuckle 480kg, Dendrobium 480kg, Achyranthes 480kg, Licorice 480kg;
[0227] Add the raw material medicine to the multifunctional extraction tank, add 5 times the amount of water, heat and cook for 1.5 hours, and start timing when the temperature in the pot reaches 100°C; after filtering, the filtrate I is obtained and input into the storage tank for standby; the medicine residue is added again 3 times the amount of water is decocted for 1 hour, filtered, and combined with filtrate I to obtain filtrate II, which is discarded; the filtrate II is input into the double-effect concentrator, the temperature is controlled below 70℃, and the vacuum degree is above -0.05Mpa Heat and concentrate to 50~60℃, relative density 1.10~1.29, collect thick paste I; take thick paste I and put it in an alcohol precipitation tank, add ethanol to 60% alcohol content, stir well, let stand for more ...
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