Rice dextrinization temperature and amylose content cooperative determining method
A technology of amylose content and gelatinization temperature, which is applied in the direction of testing starch pollutants, testing food, and analyzing materials through chemical reactions. The effect of less dosage and easy operation
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Embodiment 1
[0026] Step 1: preparing a standard iodine reagent and a potassium hydroxide solution with a mass volume ratio of 1.7%;
[0027] Step 2: use brown rice calibrated according to GB / T 15683-1999 as a standard sample;
[0028] Step 3: Select 5 standard samples and 5 samples to be tested respectively, place them in the gelatinization box, add 8mL of 1.7% potassium hydroxide solution; use glass rods to arrange the rice grains in the box evenly, and not against the wall, stamped. Move the gelatinization box smoothly to an electric heating constant temperature blast drying oven at 30°C±2°C, prevent the rice grains from moving when moving the gelatinization box, keep it warm for 23-24 hours, and then take it out smoothly.
[0029] Step 4: observe the decomposition situation of the brown rice grain endosperm of the sample to be tested which has been gelatinized grain by grain, to detect the alkali digestion value of the sample, and then determine the gelatinization temperature of the r...
Embodiment 2
[0039] Step 1: preparing standard iodine reagent and a sodium hydroxide solution with a mass volume ratio of 1.5%;
[0040] Step 2: use brown rice calibrated according to GB / T 15683-1999 as a standard sample;
[0041] Step 3: Select 7 standard samples and 7 samples to be tested respectively, place them in the gelatinization box, add 10mL of 1.5% potassium hydroxide solution; use glass rods to arrange the rice grains in the box evenly, and not against the wall, stamped. Move the gelatinization box smoothly to an electric heating constant temperature blast drying oven at 30°C±2°C, prevent the rice grains from moving when moving the gelatinization box, keep it warm for 23-24 hours, and then take it out smoothly.
[0042] Step 4: observe the decomposition situation of the brown rice grain endosperm of the sample to be tested which has been gelatinized grain by grain, to detect the alkali digestion value of the sample, and then determine the gelatinization temperature of the rice;...
Embodiment 3
[0052] Step 1: prepare standard iodine reagent and the potassium hydroxide solution that mass volume ratio is 2%;
[0053] Step 2: use brown rice calibrated according to GB / T 15683-1999 as a standard sample;
[0054] Step 3: Select 10 standard samples and 10 samples to be tested respectively, place them in the gelatinization box, add 12mL of 2% potassium hydroxide solution; cover. Move the gelatinization box smoothly to an electric heating constant temperature blast drying oven at 30°C±2°C, prevent the rice grains from moving when moving the gelatinization box, keep it warm for 23-24 hours, and then take it out smoothly.
[0055] Step 4: observe the decomposition situation of the brown rice grain endosperm of the sample to be tested which has been gelatinized grain by grain, to detect the alkali digestion value of the sample, and then determine the gelatinization temperature of the rice;
[0056] Step 5: Dyeing of the standard sample and the sample to be tested: Drain the ly...
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