Polyurethane foam plastic prepared from barbadosnut oil
A technology of polyurethane foam and jatropha oil, which is applied in the field of polyurethane foam to achieve the effects of good biodegradability, abundant raw material sources and a wide range of applications
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[0062] Example 1
[0063] Take 900 g of Jatropha oil, 85.5 g of formic acid (80%), and 18 g of phosphoric acid into a 2L glass kettle, stir, drop 558 g of 27.5% hydrogen peroxide, and react at 30 to 70°C for 6 to 10 hours. After standing, the upper layer was separated; after refining, epoxy jatropha oil was obtained, and its epoxy value was detected to be 3.95% and moisture content: 0.1%.
Example Embodiment
[0064] Example 2
[0065] Take 900g of Jatropha oil and 100g of acetic acid into a 2L glass kettle, stir, add dropwise 600g of 27.5% hydrogen peroxide, react at 30-70°C for 6-10 hours, and separate the upper layer after standing; After refining, epoxy jatropha oil was obtained. It was detected that its epoxy value was 3.85% and moisture content: 0.11%.
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[0066] Example 3
[0067] 800 g of Jatropha curcas oil, 450 diisopropanolamine, and 0.2 g of sodium methoxide produced in Example 1 were added to a 2L glass kettle, stirred and raised, and the reaction temperature was controlled at 70-200° C., and the reaction time was 12 hours. 1230 g of the bio-based polyol product A is obtained, the hydroxyl value is 471 mgKOH / g, and the moisture content: 0.1%.
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