Method for extracting pectin from banana peel
An extraction method, banana peel technology, applied in the field of extracting pectin from banana peel, can solve the problems that banana peel has not been developed and utilized, imported pectin is expensive, and the production scale is small, so as to achieve shortened extraction time and good gelation Good performance and sample quality
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Embodiment 1
[0018] Weigh 10g of banana peel, crush it with a masher, add water and bathe at 80°C for 10 minutes to inactivate the enzyme, rinse repeatedly, and dry most of the water; use 37% hydrochloric acid to prepare hydrochloric acid with a pH of 2 for extraction solution; after the banana peel is pretreated, put it in a beaker, add 160ml of hydrochloric acid extract with a pH of 2, extract for 5min under the condition of microwave power 540W, filter the extract while it is hot, wash the filter residue with hot water and filter, combine the filtrate, Keep the filtrate in a constant temperature water-soluble pot at a constant temperature to 50°C, slowly add 2.5g of aluminum sulfate, adjust the pH value to about 4 with 30% ammonia water, and place the precipitate for 1 hour to centrifugally filter, wash and drain the precipitate, and crush it. Treat with acidified ethanol, stir fully to replace the metal ions completely, and then use G3 sand core funnel to suction filter and wash the pre...
Embodiment 2
[0020] Weigh 10g of banana peel, crush it with a masher, add water and bathe at 80°C for 10 minutes to inactivate the enzyme, rinse repeatedly, and dry most of the water; use 37% hydrochloric acid to prepare hydrochloric acid with a pH of 2 for extraction liquid; after pretreatment, put it in a beaker, add 160ml of hydrochloric acid extract with a pH of 2, extract under the condition of microwave power 540W for 6min, filter the extract while it is hot, wash the filter residue with hot water and filter, combine the filtrate, and filter the filtrate Keep the temperature in a constant temperature water-soluble pot to 50°C, slowly add 2.5g of aluminum sulfate, adjust the pH value to about 4 with 30% ammonia water, and place the precipitate for 1 hour for centrifugal filtration, wash and drain the precipitate, crush it, and use acidification Ethanol treatment, fully stirred to completely replace the metal ions, and then use G3 sand core funnel to suction filter and wash the precipit...
Embodiment 3
[0022] Weigh 10g of banana peel, crush it with a masher, add water and bathe at 80°C for 10 minutes to inactivate the enzyme, rinse repeatedly, and dry most of the water; use 37% hydrochloric acid to prepare hydrochloric acid with a pH of 1 for extraction liquid; after pretreatment, put it in a beaker, add 160ml of hydrochloric acid extract with a pH of 1, extract under the condition of microwave power 540W for 6min, filter the extract while it is hot, wash the filter residue with hot water and filter, combine the filtrate, and filter the Keep the temperature in a constant temperature water-soluble pot to 50°C, slowly add 2.5g of aluminum sulfate, adjust the pH value to about 4 with 30% ammonia water, and place the precipitate for 1 hour for centrifugal filtration, wash and drain the precipitate, crush it, and use acidification Ethanol treatment, fully stirred to completely replace the metal ions, and then use G3 sand core funnel to suction filter and wash the precipitate repea...
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