Mosquito-proof finishing agent and preparation method and its uses in mosquito-preventing fabric
A technology of anti-mosquito finishing agent and anti-mosquito fabric, which is applied in fiber treatment, textiles and papermaking, etc. It can solve the problems of poor washing resistance and achieve the effects of good washing resistance, not easy to be lost, and a wide range of applications
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Embodiment 1
[0053] 1. Preparation of liquid anti-mosquito finishing agent:
[0054] (1) select raw material by following weight parts:
[0055] B-Cyclodextrin 30.0
[0056] Permethrin 2.0
[0057] Surfactant Tween-80 0.5
[0058] Ethanol 20.0
[0059] water 200.0
[0060] Citric acid 0.1
[0061] Disodium hydrogen phosphate 2.6
[0063] Imidazole resin 15.0
[0064] (2) Dissolving citric acid and disodium hydrogen phosphate in water with a total weight of 98% at normal temperature and pressure to prepare a buffer solution;
[0065] (3) Dissolving β-cyclodextrin in a buffer solution to obtain a cyclodextrin buffer solution;
[0066] (4) Mix permethrin, Tween-80, ethanol, and water with a total weight of 2% to prepare a mosquito repellent dispersion;
[0067] (5) Add the mosquito repellent dispersion liquid dropwise to the cyclodextrin buffer solution, and perform an inclusion reaction at 25.0°C for 12.0 hours to obtain a cyclodextrin / mosquito repel...
Embodiment 2
[0074] 1. Preparation of solid mosquito repellent finishing agent:
[0075] (1) select raw material by following weight parts:
[0076] Dimethyl β-cyclodextrin 30.0
[0077] β-cyclodextrin, 20.0
[0078] Permethrin 3.0
[0079] Surfactant Tween-80 0.5
[0080] Surfactant Tween-60 0.5
[0081] Acetone 30.0
[0082] water 250.0
[0083] Phosphoric acid 1.0
[0084] Sodium hydrogen phosphate 3.6
[0085] Magnesium chloride 10.0
[0086] Imidazole resin 20.0
[0087] (2) under normal temperature and pressure, phosphoric acid and sodium hydrogen phosphate are dissolved in water with a total weight of 94% to prepare a buffer solution;
[0088] (3) Dissolving β-cyclodextrin and dimethyl β-cyclodextrin in a buffer solution to obtain a cyclodextrin buffer solution;
[0089] (4) Mix permethrin, Tween-80, Tween-60, acetone, and water with a total weight of 4% to prepare a mosquito repellent dispersion;
[0090] (5) Add the mosquito repellent dispersion liquid dropwise to the ...
Embodiment 3
[0097] 1. Preparation of liquid anti-mosquito finishing agent:
[0098] (1) select raw material by following weight parts:
[0099] Hydroxyethyl-β-cyclodextrin 55.0
[0100] DEET 2.0
[0101] Permethrin 3.0
[0102] Surfactant Tween-80 0.25
[0103] Surfactant Tween-60 0.25
[0104] Surfactant Span-60 0.5
[0105] Ethanol 25.0
[0106] Acetone 20.0
[0107] water 250.0
[0108] Acetic acid 2.0
[0109] Sodium acetate 6.5
[0110] Magnesium chloride 12.0
[0111]Imidazole resin 30.0
[0112] (2) Dissolve acetic acid and sodium acetate in water (92% of the total weight) at normal temperature and pressure to prepare a buffer solution;
[0113] (3) dissolving hydroxyethyl-β-cyclodextrin in a buffer solution to obtain a cyclodextrin buffer solution;
[0114] (4) Mix and stir permethrin, DEET, surfactant Tween-80, Tween-60, Span-60, ethanol, acetone, water (8% of the total weight) evenly to prepare mosquito repellent dispersion;
[0115] (5) Add the mosquito repellent ...
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