Preparation for water chestnut leather activated char
A technology of activated carbon and water chestnut, applied in the field of preparation of water chestnut skin activated carbon, can solve the problems of high risk, difficulty in centralized collection, and environmental pollution, and achieve the effects of low environmental pollution, reduced preparation cost, and easy collection
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Embodiment 1
[0033] Water chestnut skin is dried in oven at 105 ℃ or air-dried naturally, then pulverizes, makes it pass through the sieve of 80 meshes, is that the peracetic acid of volume fraction is 30% and carries out pre-oxidation again, soaking time is 9 hours; Pour the used peracetic acid into a designated container, then soak the water chestnut skin with distilled water for 10 hours, then wash with distilled water until the pH is 6.0, and dry at 105°C; Ratio (the ratio of phosphoric acid to water chestnut powder mass) is 1.8:1 impregnation ratio impregnation 16 hours, then puts the water chestnut leather that impregnates in the muffle furnace, carbonizes at 390 ℃, activates 90 minutes, takes out after cooling to normal temperature, Wash with distilled water until the pH is 6.5, and then dry at 105°C to obtain powdered water chestnut skin activated carbon.
Embodiment 2
[0035] Water chestnut skin is dried in oven at 120 ℃ or air-dried naturally, then pulverizes, makes it pass through 100 mesh sieves, is that the peracetic acid of volume fraction is 60% and carries out pre-oxidation again, soaking time is 5 hours; Pour the used peracetic acid into a designated container, then soak water chestnut skin with distilled water for 12 hours, then wash with distilled water until the pH is 6.5, and dry at 120°C; pre-oxidize the particles with 45% phosphoric acid Ratio (the ratio of phosphoric acid to water chestnut powder mass) is 2.0:1 impregnation ratio impregnation 10 hours, then puts the water chestnut skin soaked in the muffle furnace, carbonizes at 430 ℃, activates for 70 minutes, takes out after cooling to normal temperature, Wash with distilled water until the pH is 7.0, and then dry at 120°C to obtain powdered water chestnut skin activated carbon.
Embodiment 3
[0037] The skin of water chestnut is dried in oven at 110 ℃ or air-dried naturally, then pulverizes, makes it pass through 90 mesh sieves, is soaked and carried out pre-oxidation with the peracetic acid of 45% volume fraction again, soaking time is 7 hours; Pour the used peracetic acid into a designated container, then soak water chestnut skin with distilled water for 11 hours, then wash with distilled water until the pH is 6.3, and dry at 115 ° C; Ratio (the ratio of phosphoric acid to water chestnut powder mass) is 1.9: 1 impregnation ratio impregnation 13 hours, then puts the water chestnut skin soaked in the muffle furnace, carbonizes at 410 ℃, activates 80 minutes, takes out after cooling to normal temperature, Wash with distilled water until the pH is 6.7, and then dry at 115°C to obtain powdered water chestnut skin activated carbon.
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