Supported optical catalyst preparation method

A photocatalyst and load-type technology, applied in chemical instruments and methods, physical/chemical process catalysts, chemical/physical processes, etc., can solve the problems of poor benzene removal effect, avoid secondary pollution, realize in-situ regeneration, The effect of increasing the service life

Inactive Publication Date: 2010-06-02
刘守新 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The purpose of the present invention is to solve the problem of poor benzene removal effect of the current photocatalyst, and provide a preparation method of a loaded photocatalyst

Method used

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  • Supported optical catalyst preparation method
  • Supported optical catalyst preparation method
  • Supported optical catalyst preparation method

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Experimental program
Comparison scheme
Effect test

specific Embodiment approach 1

[0013] Specific implementation mode 1: The supported photocatalyst in this implementation mode is loaded with 1 to 5 layers of TiO on the surface 2 Granular activated carbon fibers.

[0014] SEM image of activated carbon fiber figure 1 shown.

[0015] The specific surface area of ​​the activated carbon fiber used in this embodiment is 800-1500m 2 / g, the total pore volume is 0.35~0.65m 2 / g, the aperture is

specific Embodiment approach 2

[0016] Specific embodiment two: the difference between this embodiment and specific embodiment one is: the surface-loaded TiO 2 The particle size of the particles is 10-13 nm. Others are the same as the first embodiment.

[0017] After testing the TiO in this embodiment 2 The particle diameter is 10-13nm, and the critical size is 13nm, so it has high activity.

specific Embodiment approach 3

[0018] Specific embodiment three: the difference between this embodiment and specific embodiment one is: the supported photocatalyst is that the surface is loaded with 2 layers of TiO 2 Granular activated carbon fibers. Others are the same as the first embodiment.

[0019] image 3 It is a scanning electron micrograph of the supported photocatalyst in this embodiment, and the surface of the supported photocatalyst is dense and smooth.

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Abstract

The invention provides a supported photocatalyst and a preparation method thereof, relating to a photocatalyst and a preparation method thereof; the invention solves the problem of poor benzene removal effect of the existing photocatalyst. The supported photocatalyst is the active carbon fiber with TiO2 particles loaded on the surface. The catalyst has the preparation method that: 1. preparing solution A; 2. preparing solution B; 3. preparing and aging a titanium dioxide sol; 4. coating the titanium dioxide sol on the active carbon fiber, irradiating with microwaves, shifting to high purity nitrogen for purging, rising the temperature to 200-250 DEG C, keeping the temperature for 1-2h, heating to 350-450 DEG C, calcining at the constant temperature for 2-3h, and cooling to the room temperature. The supported photocatalyst of the invention has more than 28 percent of benzene removal efficiency under the condition of 30-70 DEG C and 1h of lighting, which is free from the influence of thebenzene concentration in a gaseous environment, and can completely decompose the volatile organic compounds in an enclosed environment into non-toxic, harmless and tasteless substances after a periodof time of application.

Description

technical field [0001] The invention relates to a preparation method of a photocatalyst. Background technique [0002] In recent years, with the use of indoor building decoration materials and household chemicals, indoor air pollution has become more and more serious. Paints, paints, and plywood used in living rooms and offices can release volatile organic compounds (VOCs) such as formaldehyde and benzene into the air. etc. cause indoor pollution, seriously endanger people's health, especially have carcinogenicity, and have become the most important factor causing leukemia in infants and young children. The use of photocatalysts to remove indoor volatile organic compounds is the most effective way, which can avoid the secondary pollution caused by the saturation of adsorbents, and is environmentally friendly and energy-saving; however, the current photocatalysts have poor removal effects on volatile organic compounds, especially molecular Benzene is structurally stable and ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J21/06B01J21/18A61L9/22
Inventor 刘守新刘正锋
Owner 刘守新
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