Radix astragali medicinal materials, intermediate body and method for testing fingerprint of formulation thereof as well as standard fingerprint
A detection method and fingerprint technology, applied in the field of drug quality control, can solve the problems of insufficient guarantee of the quality and efficacy of Huangqi granules
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Embodiment 1
[0052] This embodiment is the fingerprint spectrum detection method to 3 batches of Radix Astragali medicinal materials and the fingerprint spectrum obtained accordingly:
[0053] The detection method comprises the following main steps:
[0054] (1) Preparation of reference substance solution:
[0055] Weigh the reference substance of forbistin, put it in a volumetric flask, add methanol to dissolve and dilute to make a solution containing 0.1mg per 1ml, shake well to get the reference substance solution;
[0056] (2) Preparation of the test solution:
[0057] Weigh 2.0g of 3 batches of Radix Astragali (batches: 060530, 060827, and 070202) powder respectively, add 50ml of 80%, 90%, and 95% methanol, respectively, ultrasonically treat for 50min, 30min, and 20min, filter, and respectively Wash the filter residue, filter paper and funnel with an appropriate amount of methanol of the same concentration, merge the washing liquid into the filtrate, and evaporate it to dryness on a...
Embodiment 2
[0069] Present embodiment is to the fingerprint spectrum detection method of 3 batches of intermediates (Astragalus extractum) and the fingerprint spectrum obtained accordingly:
[0070] The detection method comprises the following main steps:
[0071] (1) Preparation of reference substance solution:
[0072] Weigh the reference substance of forbistin, put it in a volumetric flask, add methanol to dissolve and dilute to make a solution containing 0.1mg per 1ml, shake well to get the reference substance solution;
[0073] (2) Preparation of the test solution:
[0074] Weigh 5.0 g of 3 batches of astragalus intermediates (Astragalus extract; batches are: M070601, M070701, and M070702) respectively, put them in 25ml measuring bottles, add appropriate amounts of 80%, 90%, and 95% methanol respectively, and ultrasonically treat them for 20 minutes , 30min, and 40min, respectively add the same concentration of methanol to the scale, shake well, filter with a microporous membrane (...
Embodiment 3
[0084] This embodiment is the fingerprint detection method to 3 batches of preparations (Astragalus granules, sugar type) and the fingerprint spectrum obtained accordingly:
[0085] The detection method comprises the following main steps:
[0086] (1) Preparation of reference substance solution:
[0087] Weigh the reference substance of forbistin, put it in a volumetric flask, add methanol to dissolve and dilute to make a solution containing 0.1mg per 1ml, shake well to get the reference substance solution;
[0088] (2) Preparation of the test solution:
[0089] Take Radix Astragali preparation (Astragali granules, with glycoforms; batch numbers are: 070601, 070701, 070702), grind finely, weigh 3.0g, put it in a 50ml measuring bottle, add appropriate amount of 80%, 90%, 95% methanol respectively, Ultrasonic treatment for 20min, 30min, 50min, wash the filter residue, filter paper and funnel with an appropriate amount of methanol of the same concentration, put the washing liqu...
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