Medicaments composite for treating gland hyperplasia and breast cancer and preparation method thereof
A technique for mammary gland hyperplasia and composition, which is applied to traditional Chinese medicine compositions and substances for treating breast disease and preparation thereof, granules for breast cancer and preparation thereof, and the field of treating mammary gland hyperplasia, which can solve the problem of unreasonable preparation process and limiting curative effect of drug prescriptions, etc. question
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experiment example 1
[0024] Experimental example 1. Optimum experiment of the extraction process of the traditional Chinese medicine group and substance of the present invention
[0025] 1. Test materials
[0026] Agilent1100 high performance liquid chromatograph, including G1311A quaternary gradient pump, G1313A autosampler, G1315A diode array detector (HP, USA); Lambda 25UV / VIS spectrometer (PerkinElmer, USA); AG285 analytical balance (Mettler, Germany) Company); KS-600D ultrasonic cleaning machine (Ningbo Kesheng Instrument Factory); 98-1-B electronic thermostat heating mantle (Tianjin Test Instrument Co., Ltd.). 5-Hydroxymethylfurfural reference substance (batch number: 111626-200402), purchased from the National Institute for the Control of Pharmaceutical and Biological Products, acetonitrile chromatographically pure, and the rest of the reagents are analytical pure.
[0027] 2. Methods and results
[0028] 2.1 Determination of 5-hydroxymethylfurfural content by HPLC
[0029] 2.1.1 Chromatographic co...
experiment example 2
[0050] Experimental example 2. Screening of auxiliary materials in the preparation of capsules and granules of the present invention
[0051] The extract of the present invention contains more hygroscopic substances such as mucus and lipopolysaccharide, and the solid preparation of the product obtained is easy to absorb moisture during storage, which makes the product quality unstable; in addition, in order to make the product content accurate and convenient to take, The appropriate excipients are selected according to the hygroscopicity, moldability, melting properties, bulk density and angle of repose of the granules after mixing the excipients with the extract powder. Experimental method: Take 43.8g of comfrey, 175g of rehmannia, 45.8g of aconite (manufactured), 58.3g of corydalis, 58.3g of cinnamon, and extract and concentrate the medicinal materials according to the optimal extraction process. 43.7g of comfrey, Gourd 175g, turtle shell 87.5g, and scorpion 35g are crushed int...
experiment example 3
[0097] Experimental example 3. Preparation of the tablet of the present invention
[0098] Take one-half of the prescription amount of the above comfrey, pulverize melon, turtle, and scorpion into fine powder to obtain the fine powder of medicine for use; the other medicinal flavors are decocted in water, combined with the decoction, concentrated into an extract, mixed with the above fine powder , Then mix with 0.5-5% sodium carboxymethyl starch to obtain a drug mixture; after deerhorn gum is added to the above mixture, it is made into granules, dried, granulated, compressed, and coated to obtain .
[0099] The disintegration of the tablets made by the present invention is not good, so we screened the added disintegrants through experiments. The test results are as follows: Table 12: Table 12 Experimental results of different disintegrants made into tablets
[0100] Disintegrant
[0101] Therefore, the present invention selects sodium carboxymethyl starch as the disintegrant.
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