Pigment dispersion composition, photocurable composition, color filter and manufacture method thereof, liquid crystal display element and solid imaging element
A pigment dispersion and composition technology, which is applied in the field of photocurable compositions and pigment dispersion compositions, can solve the problems of large molecular weight, cannot be added in large quantities, cannot be introduced, etc., and achieves the effect of good color characteristics
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[0350] In preparation of the alkali-soluble resin, for example, a method by a known radical polymerization method can be employed. Various polymerization conditions such as temperature, pressure, the type and amount of the radical initiator, the type of solvent, etc. when preparing the alkali-soluble resin by the radical polymerization method can be easily set by those skilled in the art. Conditions can be determined experimentally.
[0351] As the linear organic high molecular polymer, a polymer having a carboxylic acid in a side chain is preferable. For example, in the publications of JP-A No. 59-44615, No. 54-34327, No. 58-12577, No. 54-25957, No. 59-53836, and No. 59-71048 Methacrylic acid copolymers, acrylic acid copolymers, itaconic acid copolymers, crotonic acid copolymers, maleic acid copolymers, partially esterified maleic acid copolymers, etc., as described in Acidic cellulose derivatives, polymers obtained by addition of polymers having hydroxyl groups and acid an...
Embodiment 1—1
[0546] Modulation of processed pigments
[0547] 50 g of Pigment C.I. Pigment Green 36, 500 g of sodium chloride, and 100 g of diethylene glycol were put into a stainless steel 1-gallon kneader (manufactured by Inoue Seisakusho), and kneaded for 9 hours. Next, this mixture was added to about 3 liters of water, stirred with a high-speed mixer for about 1 hour, filtered, washed with water, and dried to remove sodium chloride and solvent to obtain a processed pigment coated with a polymer compound.
[0548] Preparation of Pigment Dispersion Composition
[0549] Components of the following composition (1) were mixed, stirred and mixed at a rotation speed of 3000 rpm for 3 hours using a homogenizer, and a mixed solution containing a pigment was prepared.
[0550] composition (1)
[0551] ·Processed pigment (particle size 30nm) 95 parts
[0552] · Pigment derivative A (the following structural formula) 5 parts
[0553] Dispersant (100 parts of 30% 1-methoxy of polymer 1-1
[05...
Embodiment 1—2~1—13
[0559] Embodiment 1-2~1-13, comparative example 1-1~1-2
[0560] Except that the composition of the pigment dispersion composition obtained in Example 1-1 was changed to that described in Table 2, the others were carried out in the same manner as in Example 1-1 to obtain Examples 1-2 to 1-13 and Comparative Example 1-1-1-2 pigment dispersion composition.
[0561] Embodiment 1-14~1-18, comparative example 1-3~1-4
[0562] Except adding 25 g of the high molecular compound (polymer) solution described in Table 2 to 50 g of Pigment C.I. Pigment Green 36, 500 g of sodium chloride, and 100 g of diethylene glycol, it was prepared in the same manner as in Example 1-1.
[0563] Evaluation of Pigment Dispersion Compositions
[0564] The following evaluations were performed on the obtained pigment dispersion composition. The results are shown in Table 2.
[0565] (1) Measurement and evaluation of viscosity
[0566] For the obtained pigment dispersion composition, the viscosity η of ...
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