Rubber ferromagnetic oxide powder and preparation method thereof
A ferrite magnet, rubber and plastic technology, applied in the direction of magnets, magnetic objects, electrical components, etc., can solve the problems of high production cost, magnetic powder particle size, inability to meet performance requirements, poor mechanical properties of magnetic strips, etc., to achieve control of grain growth , high magnetic properties, good mechanical properties
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Embodiment 1
[0035] Mix 500g of iron red with a purity of 98.5%, APD of 0.8μm, and a Cl content of 0.5% with 108g of barium carbonate with a purity of 98.8%, and add 1.2g of SiO 2 , 3.6g CaCO 3 and 10gSrCl 2 ·6H 2 O, use a vibrating mill to mix and make a mixture.
[0036]After pelletizing the mixture with water, use an electric furnace to sinter at 1150°C for 2 hours. After cooling, use a dry ball mill to coarsely crush until the APD is about 2.8 μm, and then use a ball mill to wet finely grind (the mass of coarse powder and water The ratio is about 0.5-1:1) to APD about 1.4μm, dried until the water content is less than 1%, and dispersed with a high-speed pulverizer to obtain magnetic powder.
[0037] Put 15g of magnetic powder into a cylindrical mold with a diameter of 25.2mm, under the molding pressure of 1ton / cm 2 After being pressed under certain conditions, the measured compressive density (CD) value is 3.04g / cm 3 .
[0038] After heating and mixing 16.4g of the above-mentioned...
Embodiment 2
[0040] Mix 500 g of iron red with a purity of 98.5%, an APD of 0.8 μm, and a Cl content of 0.5%, with 81 g of strontium carbonate with a purity of 97.9%, and add 1.1 g of SiO 2 , 3.5gCaCO 3 and 5g SrCl 2 ·6H 2 O, use a vibrating mill to mix and make a mixture.
[0041] After the mixture is pelletized with water, it is sintered at 1120°C for 2 hours using an electric furnace. After cooling, use a dry ball mill to coarsely crush until the APD is 3.1 μm, then use a ball mill to wet finely grind to an APD of 1.5 μm, dry until the moisture is less than 1%, and then disperse with a high-speed pulverizer.
[0042] Put 15g of magnetic powder into a cylindrical mold with a diameter of 25.2mm, under the molding pressure of 1ton / cm 2 After being pressed under certain conditions, the measured CD value is 3.01g / cm 3 .
[0043] After heating and mixing 16.4g of the above-mentioned magnetic powder and 1.6g of paraffin wax evenly, put them into a cylindrical mold with a diameter of 25.2...
Embodiment 3
[0045] Mix 500 g of iron red with a purity of 98.5%, an APD of 0.8 μm, and a Cl content of 0.5%, and 108 g of barium carbonate with a purity of 98.8%, and add 3.2 g of CaCO 3 and 10g SrCl 2 ·6H 2 O, use a vibrating mill to mix and make a mixture.
[0046] After the mixture is pelletized with water, it is sintered at 1160°C for 2 hours using an electric furnace. After cooling, use a dry ball mill to coarsely crush until the APD is 3.0 μm, then use a ball mill to wet finely grind it to an APD of 1.5 μm, dry it until the moisture is less than 1%, and then disperse it with a high-speed pulverizer.
[0047] Put 15g of magnetic powder into a cylindrical mold with a diameter of 25.2mm, under the molding pressure of 1ton / cm 2 After being pressed under certain conditions, the measured CD value is 2.98g / cm 3 .
[0048] After heating and mixing 16.4g of the above-mentioned magnetic powder and 1.6g of paraffin wax evenly, put them into a cylindrical mold with a diameter of 25.2mm, an...
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