Method for preparing biodiesel from sugarcane
A biodiesel and sugarcane technology, applied in the preparation of biological raw materials, biofuels, liquid hydrocarbon mixtures, etc., can solve the problems of high cost and cumbersome steps, and achieve the effects of reducing production costs and simplifying the cultivation process.
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Embodiment 1
[0075] (1) Preparation of seeds: Chlorella protothecoides (Chlorella protothecoides) (purchased from the Algae Center of the University of Texas, U.S.) is cultivated in a heterotrophic medium as seeds, and the heterotrophic medium includes: 30gL -1 Glucose, 3gL -1 Yeast extract, 0.7gL -1 K H 2 PO 4 , 0.3gL -1 K 2 HPO 4 , 0.3gL -1 MgSO 4 ·7H 2 O, 0.3mgL -1 FeSO 4 ·7H 2 O, 5gL -1 Glycine and 0.01mg L -1 Vitamin B1.
[0076] (2) Obtaining sugarcane juice enzymatic hydrolysis: use a commercially available household sugarcane juicer to obtain sugarcane juice (model YZ28, brand: Henglian), which has a hydraulic device inside, integrating rolling, squeezing and collecting operations, The sugarcane juice is squeezed directly through powerful pressure.
[0077] The sugarcane juice is extracted from fresh sugarcane bought in the market and collected in a container. Under the greenhouse, add sucrose invertase (trade name Validase) to sugarcane juice Invertase ANL), the ...
Embodiment 2
[0083] Experiment with the same method as in Example 1, except that the shaking flask culture of Chlorella is replaced with the following fermentation experiments:
[0084] 5L fermentation experiment of Chlorella: Prepare a 5L fermenter (MINIF ORS, Switzerland), assemble temperature, pH, dissolved oxygen electrodes and defoaming electrodes, add 3L heterotrophic medium as described in step 3, and steam sterilize Let cool and set aside. The heterotrophic fermentation conditions are set as follows: temperature 28±1°C, aeration rate about 180L / h, pH value 6.3±0.5, stirring speed 350±50rpm; online monitoring of dissolved oxygen changes in the fermenter to keep it at 10- Within the range of 40% saturation; when the carbon source is consumed, the concentrated enzymolysis solution described in Example 2 (for ease of operation, the enzymolysis solution is preferably concentrated to a reducing sugar concentration of about 500g / L through freeze-drying) flow Add it to the fermenter to co...
Embodiment 3-7
[0086] Experiment in the same way as in Example 1, except that the initial reducing sugar concentration in the shake flask is configured as: 5gL -1 , 10gL -1 , 15gL -1 , 25gL -1 , 30gL -1 outside. From Figure 7 It can be seen that within 75 hours of culture time, Chlorella can grow in different carbon source concentration ranges, showing a certain tolerance.
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