Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Industrial novel method for synthesizing graphite fluoride

A technology of fluorinated graphite and graphite, which is applied in the petroleum industry, lubricating compositions, electrical components, etc., and can solve problems such as difficulty in increasing fluorine content, poor quality of fluorinated graphite, and low output of fluorinated graphite

Inactive Publication Date: 2009-07-22
杨先金 +2
View PDF0 Cites 21 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In general laboratories, the synthetic fluorine content can reach more than 55%, but the output of fluorinated graphite is very low, and it can only be prepared on a small scale.
Under the premise of increasing the production capacity of general industrial synthesis methods, it is difficult to increase the fluorine content, so the quality of fluorinated graphite is not good, and the production is easy to explode

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Industrial novel method for synthesizing graphite fluoride

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0008] Add 500 microns and 600 kg of graphite into the reaction vessel, spread evenly on the reaction plates of each layer, heat the reactor to a temperature of 200 to 300 degrees, vacuumize the reaction system, and remove the air from the reaction system. Raise the temperature to 500 to 600 degrees, slowly introduce fluorine gas, control the flow rate of fluorine gas added by the fluorine gas flow meter to 3 to 50 liters per minute, continue to react at this flow rate for 5 to 10 hours, stop heating, let the reaction The kettle is naturally cooled to a temperature below 300 degrees, and nitrogen gas is introduced into the cooled reaction vessel to drive away the residual fluorine gas in the reaction vessel, and the reaction ends. Open the reaction kettle, take out the solid powder in the reaction kettle according to the color classification, and obtain the product. The total weight of the product is 1500 kg, the black color is 300 kg, the fluorine content is 50% to 55%, and th...

example 2

[0010] Add graphite 50 microns and 600 kg into the reaction vessel, spread evenly on the reaction plates of each layer, heat the reactor to a temperature of 200 to 300 degrees, vacuumize the reaction system, and clean the reaction system twice. Raise the temperature to 500 to 600 degrees, slowly introduce fluorine gas, control the flow rate of fluorine gas added by the fluorine gas flow meter to 3 to 50 liters per minute, continue to react at this flow rate for 5 to 10 hours, stop heating, let the reaction The kettle is naturally cooled to a temperature below 300 degrees, and nitrogen gas is introduced into the cooled reaction vessel to drive away the residual fluorine gas in the reaction vessel, and the reaction ends. Open the reaction kettle, take out the solid powder in the reaction kettle according to the color classification, and obtain the product. The total weight of the product is 1500 kg, the black color is 300 kg, the fluorine content is 50% to 55%, and the gray to of...

example 3

[0012] Add graphite 10 microns and 600 kg into the reaction vessel, spread it evenly on the reaction plates of each layer, heat the reactor to a temperature of 200 to 300 degrees, vacuumize the reaction system, and remove the air from the reaction system. Raise the temperature to 500 to 600 degrees, slowly introduce fluorine gas, control the flow rate of fluorine gas added by the fluorine gas flow meter to 3 to 50 liters per minute, continue to react at this flow rate for 5 to 10 hours, stop heating, let the reaction The kettle is naturally cooled to a temperature below 300 degrees, and nitrogen gas is introduced into the cooled reaction vessel to drive away the residual fluorine gas in the reaction vessel, and the reaction ends. Open the reaction kettle, take out the solid powder in the reaction kettle according to the color classification, and obtain the product. The total weight of the product is 1500 kg, the black color is 300 kg, the fluorine content is 50% to 55%, and the...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses an industrial synthesis method for graphite fluoride. Fluorine gas or the mixture of fluorine gas and inert gas is led into a specific reaction container filled with graphite at certain flow speed and pressure; and then graphite fluoride with various specifications of more than 50 percent is obtained by controlling reaction temperature, reaction pressure and reaction speed. Compared with methods specified in other relevant patents, the method has simple operation and can carry out industrial production safely. The obtained graphite fluoride products are mainly applied to the electrode materials of novel high-energy lithium ion battery and solid lubricant material.

Description

technical field [0001] Graphite fluoride is a solid lubricant with excellent lubricating properties, widely used in national defense, machinery, precision instruments and other fields. Background technique [0002] There are many ways to synthesize graphite fluoride, and there are relevant patent reports at home and abroad. The synthesis of graphite fluoride by different methods has its own characteristics. Generally, the synthetic fluorine content in the laboratory can reach more than 55%, but the output of fluorinated graphite is very low, and it can only be prepared on a small scale. Under the premise of increasing the production capacity of general industrial synthesis methods, it is difficult to increase the fluorine content, so the quality of fluorinated graphite is not good, and the production is easy to explode. Contents of the invention [0003] The invention provides an industrial synthesis method of fluorinated graphite, which can produce fluorinated graphite ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C01B31/00H01M4/58C10M103/00
CPCY02E60/10
Inventor 杨先金朱耀平王莹杨明杰徐剑张建设
Owner 杨先金
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com