Method for preparing photo-thermal curing conductive slurry
A technology of conductive paste and photothermal curing, which is applied in the manufacture of cables/conductors, conductive materials dispersed in non-conductive inorganic materials, circuits, etc., can solve the problems of long drying time, affecting work efficiency, high cost and price, and achieves Low cost, improved production efficiency, and increased printing resolution
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Embodiment 1
[0011] A kind of preparation of photothermal curing conductive paste, comprises the following steps:
[0012] 1) Select 10 parts by mass of diethyl adipate as the solvent, mix with 3 parts by mass of hard polyester resin VITEL PE-708 and soft polyester resin VITEL R60B, wherein 0.5 parts of hard polyester resin Stir and mix polyester resin VITEL PE-708 and 2.5 parts of soft polyester resin VITEL R60B at 60°C until uniform;
[0013] 2) In the above mixture, add 9 parts by mass of polyester acrylate UCB-657, add 9 parts by mass of reactive diluent isobornyl acrylate, stir and mix;
[0014] 3) In the above mixture, add photoinitiator DAROCUR-1173, 0.5 parts of light stabilizer TINUVIN-292, 0.5 parts of activator triethanolamine according to 0.5 parts by mass, add 0.5 parts of dispersant BYK-104, at room temperature Stir to mix;
[0015] 4) In the above mixture, add flake silver powder with a particle diameter of 5 μm and a tap density of 1.5 to 4.0 g / ml according to 50 parts by...
Embodiment 2
[0018] A kind of preparation of photothermal curing conductive paste comprises the following steps:
[0019] 1) Select 15 parts by mass of diethyl adipate as the solvent, mix with 8 parts by mass of hard polyester resin VITEL PE-708 and soft polyester resin VITEL R60B, wherein hard polyester resin 2 parts of VITEL PE-708, 6 parts of soft polyester resin VITEL R60B, stirring and mixing at 60°C until uniform;
[0020] 2) In the above mixture, add 17 parts by mass of polyester acrylate PE-56F, add 20 parts by mass of reactive diluent isooctyl acrylate, stir and mix;
[0021] 3) In the above mixture, add photoinitiator DAROCUR-1173, light stabilizer TINUVIN-292, 1.5 parts of activator triethanolamine in 3 parts by mass, add 1.5 parts of dispersant BYK-161, stir and mix at room temperature ;
[0022] 4) In the above mixture, add flake silver powder with a particle diameter of 10 μm and a tap density of 1.5 to 4.0 g / ml according to 70 parts by mass, and stir and mix;
[0023] 5) ...
Embodiment 3
[0025] A kind of preparation of photothermal curing conductive paste comprises the following steps:
[0026] 1) Select 8 parts by mass of 1,4-butyrolactone as a solvent, mix with 7 parts by mass of hard polyester resin VITEL PE-708 and soft polyester resin VITEL R60B, wherein hard polyester Resin VITEL PE-708 is 2 parts, soft polyester resin VITEL R60B is 5 parts, stir and mix at 60°C until uniform;
[0027] 2) In the above mixture, add 13 parts by mass parts of aliphatic urethane acrylate B-618, add 8 parts by mass parts of reactive diluent isobornyl acrylate, stir and mix;
[0028] 3) Add 1.5 parts by mass of photoinitiator DAROCUR-1173, 0.5 parts by mass of light stabilizer TINUVIN-292, 1.5 parts of activator triethanolamine, and 0.5 parts of dispersant Noveon in the above mixture. Stir and mix at room temperature;
[0029] 4) In the above mixture, add flake silver powder with a particle diameter of 15 μm and a tap density of 1.5 to 4.0 g / ml according to 59 parts by mass,...
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