Leaching method for anode material of waste LiCoO battery
A cathode material and waste battery technology, which is applied in the field of leaching cathode materials of lithium cobalt oxide waste batteries, can solve the problems of large nitrogen oxides, pollute the environment, large consumption of nitric acid, etc., and achieve the reduction of consumption of nitric acid, obvious economic benefits and Environmental benefits, the effect of saving pollution control costs
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Embodiment 1
[0022] Example 1: 100g of lithium cobalt oxide waste battery positive electrode material (containing 53.6% of cobalt, 5.3% of lithium, 8.2% of copper, and 3.4% of aluminum) is added in a stainless steel autoclave with a volume of 2L, and 1800ml of nitric acid of 3.0mol / L is added, Introduce 0.2MPa industrial pure oxygen, stir at 40-50°C (stirring speed 80r / min) for leaching for 2.5 hours, perform liquid-solid separation after leaching, and obtain 1750ml leaching solution (excluding leaching slag washing water). The reaction tail gas is about 600ml (converted into a volume with an absolute pressure of 0.1MPa), and the concentration of nitrogen oxides is 7.3mg / m 3 . The leaching rates of cobalt, lithium and copper are respectively 98.3%, 98.5% and 97.9% (calculated according to the cobalt, lithium and copper entering the leaching solution and leaching slag washing liquid).
Embodiment 2
[0023] Embodiment 2: 400g nickel metal hydride waste battery cathode material (containing cobalt 53.6%, lithium 5.3%, copper 8.2%, aluminum 3.4%) is added in the stainless steel autoclave that volume is 10L, adds the nitric acid 8.5L of 2.5mol / L, Introduce industrial pure oxygen of 0.1MPa, stir at 50-60°C (stirring speed 80r / min) for 3 hours, carry out liquid-solid separation after leaching, obtain 8.4L leaching solution (excluding leaching slag washing water), and react The exhaust gas is about 3.2L (converted into a volume with an absolute pressure of 0.1MPa), and the concentration of nitrogen oxides is 6.7mg / m 3 . The leaching rates of cobalt, lithium and copper are respectively 98.1%, 98.2% and 97.6% (calculated according to the cobalt, lithium and copper entering the leaching solution and leaching slag washing liquid).
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