Method for deeply drying gas
A technology for drying and raw gas, applied in separation methods, chemical instruments and methods, dispersed particle separation, etc., can solve the problems of difficult regeneration, waste of regeneration energy consumption, etc.
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Embodiment 1
[0014] Example 1: The hydrogen concentration of a certain gas is 99.9%, the water vapor content is 20°C dew point, and the dew point needs to be lowered to below -70°C.
[0015] After compression to a pressure of 0.3MPa (table), after pre-purification, the mechanical water component in the gas is removed to become the raw material gas. Two adsorption towers are installed, one of which passes the raw material gas, and the gas concentration at the outlet of the adsorption tower is from dew point to -70 Below ℃, another tower is used to regenerate the adsorbent. The two towers are operated alternately to obtain qualified purified gas.
[0016] Each adsorption tower is equipped with three layers of adsorbents, the first layer is 1 / 3 of activated alumina, the second layer is 1 / 3 of silica gel, and the third layer is 1 / 3 of 13X molecular sieve.
[0017] In the regeneration state of the adsorption tower, the front-stage adsorbent can desorb most of the adsorbed water through the dep...
Embodiment 2
[0018] Example 2: A gas with a carbon monoxide concentration of 99.99% and a water vapor content of 100 ppm needs to reduce the water vapor to below 1 ppm.
[0019] After being compressed to a pressure of 0.1MPa (table), two adsorption towers are set, one of which passes through the feed gas, the gas concentration at the outlet of the adsorption tower is below 1ppm, and the other tower is used to regenerate the adsorbent.
[0020] Each adsorption tower is equipped with two layers of adsorbent, the first layer is 2 / 3 of activated alumina, and the second layer is 1 / 3 of 13X molecular sieve.
[0021] In the regeneration state of the adsorption tower, the front-stage adsorbent can desorb most of the adsorbed water through the depressurization process, and at the same time, the dried purified gas is used to purge the heated 13X molecular sieve layer, so that the water adsorbed by the 13X molecular sieve layer is gradually desorbed, while The outflowing purge gas directly continues ...
Embodiment 3
[0022] Example 3: A certain gas has a methane concentration of 99% and a water vapor content of 1%. It is necessary to reduce the water vapor to below 0.05%.
[0023] After being compressed to a pressure of 1.0MPa (table), three adsorption towers are set, one of which passes through the feed gas, the gas concentration at the outlet of the adsorption tower is below 0.05%, and the other two towers are used to regenerate the adsorbent.
[0024] Each adsorption tower is equipped with two layers of adsorbent, the first layer is 2 / 3 of silica gel, and the second layer is 1 / 3 of 5A molecular sieve.
[0025] In the regeneration state of the adsorption tower, the adsorbent in the front stage can desorb most of the adsorbed water through the depressurization process, and at the same time, the dried purified gas is used to purge the heated 5A molecular sieve layer, so that the water adsorbed by the 5A molecular sieve layer is gradually desorbed, while The outflowing purge gas directly co...
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