Method for preparing powder of nanometer tantalum carbide
A nano-tantalum carbide and powder technology is applied in the field of non-metallic materials, which can solve the problems of high energy consumption, inability to prepare nano-tantalum carbide powder, and high investment cost, and achieve the effects of low energy consumption, solving preparation problems and small equipment investment.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0030] In this embodiment, 1.00 g of tantalum pentachloride is placed in a beaker, 10 ml of absolute ethanol is added to the beaker and stirred evenly with a glass rod, then the beaker is placed in an ultrasonic cleaner, and the heating temperature is set to 55°C , the operating frequency is 40kHz, the ultrasonic power is 80W, after ultrasonic oscillation for 5 minutes, a liquid phase precursor is made, and 0.20 g of activated carbon powder with a particle size of 24 nanometers is added to the liquid phase precursor, and ultrasonic oscillation is continued for 20 minutes;
[0031] Transfer the mixed liquid to a 95 porcelain crucible, and distribute it on the inner wall of the crucible as evenly as possible, and dry it slowly with a hot air blower;
[0032] Put the crucible into a vacuum furnace, perform high-temperature treatment on it under a vacuum of 100 Pa, the heating rate is 20°C / min, heat up to 1300°C for 0.5 hours, and cool with the furnace; take out the crucible, and u...
Embodiment 2
[0035] In this embodiment, 1.00 g of tantalum pentachloride is placed in a beaker, 20 ml of absolute ethanol is added to the beaker and stirred evenly with a glass rod, then the beaker is placed in an ultrasonic cleaner, and the heating temperature is set to 65°C , the operating frequency is 40kHz, the ultrasonic power is 90W, after ultrasonic oscillation for 8 minutes, a liquid phase precursor is made, and 0.40 g of activated carbon powder with a particle size of 24 nanometers is added to the liquid phase precursor, and ultrasonic oscillation is continued for 30 minutes;
[0036] Transfer the mixed liquid to a 95 porcelain crucible, and distribute it on the inner wall of the crucible as evenly as possible, and dry it slowly with a hot air blower;
[0037] Put the crucible into a vacuum furnace, carry out high-temperature treatment on it under a vacuum of 100 Pa, the heating rate is 15°C / min, heat it up to 1200°C for 4 hours, and cool down with the furnace; take out the crucibl...
Embodiment 3
[0040] In this embodiment, 0.50 g of tantalum pentachloride is placed in a beaker, 5 ml of absolute ethanol is added to the beaker and stirred evenly with a glass rod, then the beaker is placed in an ultrasonic cleaner, and the heating temperature is set to 50°C , the operating frequency is 40kHz, the ultrasonic power is 85W, after ultrasonic oscillation for 3 minutes, a liquid phase precursor is made, and 0.10 g of activated carbon powder with a particle size of 24 nanometers is added to the liquid phase precursor, and ultrasonic oscillation is continued for 15 minutes;
[0041] Transfer the mixed liquid to a 95 porcelain crucible, and distribute it on the inner wall of the crucible as evenly as possible, and dry it slowly with a hot air blower;
[0042] Put the crucible into a vacuum furnace, carry out high-temperature treatment on it under a hydrogen atmosphere, the heating rate is 25°C / min, heat up to 1300°C for 0.5 hours, and cool with the furnace; take out the crucible, a...
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle size | aaaaa | aaaaa |
| particle size | aaaaa | aaaaa |
| particle size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More